STRUCTURE ELUCIDATION AND NMR CHARACTERIZATION OF 5,10-DIHYDROPHENOPHOSPHAZINE DERIVATIVES

Chinese Journal of Magnetic Resonance ›› 2004, Vol. 21 ›› Issue (1): 79-85.

STRUCTURE ELUCIDATION AND NMR CHARACTERIZATION OF 5,10-DIHYDROPHENOPHOSPHAZINE DERIVATIVES

JIN Kun^1*, YIN Zhi-Gang², PENG Qi-Ji¹, ZAAO De-Feng¹

1.Dalian University of Technology，State Key Laboratory of Fine Chemicals, Dalian 116012, China; 
2.Department of Chemical Engineering, Zhengzhou Institute of Light Industry, Zhengzhou 450002, China

Received:2003-06-17 Revised:2003-08-13 Online:2004-03-05 Published:2004-03-05

The structures of thirteen 5,10-dihydrophenophosphazine derivatives were elucidated by ¹H, ¹³C and two-dimensional NMR. The ¹H and ¹³C chemical shifts were assigned, and the coupling constants between ¹⁹P and ¹H/¹³C were determined accurately. The factors affecting coupling constants were also investigated.

Key words: NMR, assignment, 5,10-dihydrophenophosphazine derivatives, coupling constant

CLC Number:

O482.53

Cite this article

JIN Kun, YIN Zhi-Gang, PENG Qi-Ji, ZAAO De-Feng. STRUCTURE ELUCIDATION AND NMR CHARACTERIZATION OF 5,10-DIHYDROPHENOPHOSPHAZINE DERIVATIVES[J]. Chinese Journal of Magnetic Resonance, 2004, 21(1): 79-85.

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References

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