Chinese Journal of Magnetic Resonance ›› 2004, Vol. 21 ›› Issue (4): 499-504.

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AN NMR STUDY OF HYODEOXYCHOLIC ACID DERIVATIVES

 LEI Xin-Xiang, ZHANG An-Jiang*, XIONG Jing, CHEN Shu-Hua, LI Ling   

  1. NMR Laboratory, Wenzhou Normal College, Wenzhou 325027, China; Faculty of Chemistry, Sichuan University, Chengdu 610064, China
  • Received:2004-04-12 Revised:2004-05-25 Online:2004-12-05 Published:2004-12-05
  • Supported by:

    教育部“高等学校骨干教师资助计划”基金 (1812), 浙江省“151”人才工程基金资助项目.

Abstract:

The structures of 3α-benzoyloxy-6α-hydroxy-5β-methyl cholanate and 6α-benzoyloxy-3α-hydroxy-5β-methyl cholanate were determined by the combination of 1D and 2D NMR techniques. The carbon and proton chemical shifts of the compounds were assigned, and the characteristics of the chemical shifts for each compound were analyzed.

Key words: NMR, chemical shift assignment, hyodeoxycholic acid

CLC Number: