Chinese Journal of Magnetic Resonance ›› 2005, Vol. 22 ›› Issue (3): 277-283.

• Articles • Previous Articles     Next Articles

Structure Elucidation of A Higher Carbon Sugar-Derived Amino Alcohol and Its Hydrolysate by NMR

  

  1. Department of Chemistry,Zhengzhou University ,Zhengzhou 450052,China
  • Received:2005-04-14 Revised:2005-06-09 Online:2005-09-05 Published:2005-09-05
  • Supported by:

    国家自然科学基金资助项目(20272054).

Abstract:

An amino alcohol and its hydrolysate, which are potential glycosidase inhibitors, were synthesized from C10 higher carbon sugar. The structures of these novel higher carbon sugar-derived compounds were elucidated by NMR. The 1H and 13C chemical shifts of the hydrolysate of the amino alcohol were completely assigned by 2D NMR techniques including 1H-1H COSY, HMQC and HMBC.

Key words: NMR, higher carbon sugar, amino alcohol, chemical shift assignment, hydrolysis

CLC Number: