波谱学杂志

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全自动式EPR样品管清洗装置的设计

李晶鑫*,童伟#,张志涛,于璐,皮雳   

  1. 极端条件凝聚态物理安徽省重点实验室,中国科学院合肥物质科学研究院强磁场科学中心,安徽 合肥 230031

  • 收稿日期:2024-06-26 修回日期:2024-07-31 出版日期:2024-08-01 在线发表日期:2024-08-01
  • 通讯作者: 李晶鑫;童伟 E-mail:jingxinli@hmfl.ac.cn;weitong@hmfl.ac.cn

Design of an automated instrument for washing EPR sample tubes

Li Jingxin*, Tong Wei#, Yu Lu, Zhang Zhitao, Pi Li   

  1. Anhui Province Key Laboratory of Condensed Matter Physics at Extreme Conditions, High Magnetic Field Laboratory, The Hefei Institutes of Physical Science, Chinese Academy of Sciences, Hefei 230031, China
  • Received:2024-06-26 Revised:2024-07-31 Published:2024-08-01 Online:2024-08-01
  • Contact: Li Jingxin;Tong Wei E-mail:jingxinli@hmfl.ac.cn;weitong@hmfl.ac.cn

摘要: 针对磁共振领域电子顺磁共振(EPR)细长样品管难清洗的问题,设计了一种全自动式EPR样品管清洗装置.整个装置主要包括纯水机、储水箱、增压水泵、空压机、控制器、电磁阀管路以及清洗台,通过树莓派电脑和继电器扩展模块以及Python GUI程序控制电磁阀和电机/升降杆实现EPR样品管的全自动式清洗及吹干.利用该装置对盛装过固体和粘稠液体的EPR样品管进行清洗效果对比,结果表明该装置清洗效果好(低温T =2 K条件下无杂质信号),效率高(5 min内完成一次清洗干燥),具有较高的实际应用价值.

关键词: 全自动, 清洗, 磁共振, EPR, 样品管

Abstract: Many quartz tubes were used in electron paramagnetic resonance (EPR) experiments. These tubes were long and thin, and difficult to be cleaned. Here, an automated washing instrument for EPR sample tubes were designed for this purpose. The whole instrument mainly includes water purification machine, water storage tank, booster pump, air compressor, controller, solenoid valve pipeline and washing rack. Fully automatic washing EPR sample tubes was achieved through the Raspberry Pi computer, relay extension module and the Python Graphical User Interface (GUI) program by controlling the solenoid valve and the motor/lifter. The cleaning effects which the EPR sample tubes contained solid and viscous liquid were compared by using this washing instrument. The results demonstrate that the washing instrument exhibit excellent cleaning effect (no impurity signals in low temperature T =2 K) and high efficiency (cleaning and drying within 5 min), and it has high practical application value.

Key words: Automated, Washing, Magnetic resonance, EPR, Sample tubes