波谱学杂志

• 研究论文 • 上一篇    下一篇

高场核磁共振波谱仪频率合成器设计

刘海丹1,2,王恢旺1,2,朱天雄1,2,宋侃 1,2,刘朝阳1*     

  1. 1. 波谱与原子分子物理国家重点实验室,武汉磁共振中心(中国科学院武汉物理与数学研究所),湖北 武汉 430071;
    2. 中国科学院大学,北京 100049
  • 收稿日期:2013-04-12 修回日期:2013-04-28 出版日期:2014-03-05 发布日期:2014-03-05
  • 作者简介:刘海丹(1987-),女,湖北人,硕士研究生,无线电物理专业.*通讯联系人:刘朝阳,电话:027-87198790,E-mail: chyliu@wipm.ac.cn.
  • 基金资助:

    国家自然科学基金资助项目(10675162),科技支撑计划资助项目(2006BAK03A22).

A Frequency Synthesizer For High-Field NMR Spectrometers

LIU Hai-dan1,2,WANG Hui-wang1,2,ZHU Tian-xiong1,2,SONG Kan1,2,LIU Chao-yang1*   

  1. 1. State Key Laboratory of Magnetic Resonance and Atomic Molecular Physics, Wuhan Center for Magnetic Resonance(Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences), Wuhan 430071, China;
    2. University of Chinese Academy of Sciences, Beijing 100049, China
  • Received:2013-04-12 Revised:2013-04-28 Online:2014-03-05 Published:2014-03-05
  • About author:*Corresponding author:LIU Chao-yang, Tel: 027-87198790, E-mail: chyliu@wipm.ac.cn.
  • Supported by:

    国家自然科学基金资助项目(10675162),科技支撑计划资助项目(2006BAK03A22).

摘要:

提出了一种基于锁相环(Phase-locked Loop, PLL)与直接数字合成(Direct Digital Synthesis, DSS)等技术相结合的高场核磁共振波谱仪频率合成器设计方案.该系统以单片机为控制器完成算法运行、参数配置和CAN 总线通信功能,运用PLL 技术和DDS 技术相结合的频率合成方案,通过两次混频,使频率粗调和细调灵活可控,实现宽带低噪声频率输出.将该频率合成器用于自主研制开发的核磁共振波谱仪上进行实验验证,测试得到的线形和灵敏度均达到指标要求,结果证明该设计方案具有可行性.

关键词: 核磁共振(NMR), 频率合成器, 锁相环, 直接数字合成, 低相位噪声

Abstract:

A frequency synthesizer based on PLL and DDS was designed for high-field NMR spectrometers. An MCU controller with CAN interface is used as the center
processor for the system, which receives instructions from the NMR console and controls the other components to change the power and frequency of the output. The PLL frequency synthesizer is used to get stable and pure signal for mixing, contributing to low phase noise and wide band spanning from 5 to 645 MHz. Combined with DDS, the resolution of the synthesizer can be as high as μHz. This design has many other benefits, including easy control, high precision and low cost.

Key words: NMR, frequency synthesizer, PLL, DDS, low phase noise

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