波谱学杂志 ›› 1992, Vol. 9 ›› Issue (2): 177-182.

• 研究论文 • 上一篇    下一篇

1,2,4,6-四苯基-2-羟基-8-氮杂双环[3、2、1]辛烷的核磁共振研究

江建平, 廖海平, 姚亦明, 高炬, 陈伟兴, 沈文斌   

  1. 南京大学化学系, 南京 210008
  • 收稿日期:1991-03-20 修回日期:1991-10-22 出版日期:1992-06-05 发布日期:2018-01-20

NMR STUDY OF 1,2,4,6-TETRAPHENYL-2-HYDROXYL-8-AZABICYCLO[3、2、1] OCTANE

Jiang Jianping, Liao Haping, Yao Yiming, Gao Ju Shen, Wenbing, Chen Weixing   

  1. Nanjing University, Nanjing 210008
  • Received:1991-03-20 Revised:1991-10-22 Online:1992-06-05 Published:2018-01-20

摘要: 用多种核磁共振实验方法并结合其它结构信息,确定1,2,4,6-四苯基-2-羟基8-氮杂双环[3、2、1]辛烷的化学结构,并指定该化合物的核磁共振归属.

关键词: 颠茄生物碱, 1,2,4,6-四苯基-2-羟基-8氮杂双环[3、2、1]辛烷, 同核二维相关谱, 异核二维相关谱, 无畸变的极化转移增强法, 核磁共振

Abstract: The chemical structure of a new synthetic product 1,2,4,6-tetraphenyl-2 -hydroxyl-8-azabicyclo[3、2、1] octane was studied and identified by various NMR spectra (including NON, SD, BB, DEPT, COSY and HETCOR).

Key words: Atrope alkaloid, 1,2,4,6-tetraphenyl-2 -hydroxyl-8-azabicyclo[3、2、1] octane, COSY, HETCOR, DEPT, NMR