[1] Schmidt-Rohr K, Spiess H W. Multidimensional Solid-State NMR and Polymers[M]. London: Academic Press, 1994.
[2] Laws D D, Bitter H M L, Jerschow A. Solid-state NMR spectroscopic methods in chemistry[J]. Angew Chem Int Edit, 2002, 41(17): 3 096-3 129.
[3] Ernst R R, Bodenhausen G, Wokaun A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions[M]. Clarendon Press: Oxford, 1987.
[4] Gao Han-bin(高汉宾), Zhang Zhen-fang(张振芳). 核磁共振原理与实验方法[M]. Wuhan(武汉):Wuhan University Press(武汉大学出版社), 2008.
[5] Tonelli A E. NMR Spectroscopy and Polymer Microstructure: The Conformational Connection[M]. Wiley-VCH, Verlag Gmbh & Co. kGaA, 1989.
[6] Clauss J, Schmidt-Rohr K, Spiess H W. Determination of domain sizes in heterogeneous polymers by solid-state NMR[J]. Acta Polym, 1993, 44(1): 1-17.
[7] Ibbett R N. NMR Spectroscopy of Polymers[M]. Blackie Academic & Professional, 1993.
[8] Griffin R G. SPECTROSCOPY clear signals from surfaces[J]. Nature, 2010, 468(7322): 381-382.
[9] Lesage A, Lelli M, Gajan D, et al. Surface enhanced NMR spectroscopy by dynamic nuclear polarization[J], J Am Chem Soc, 2010, 132(44): 15 459-15 461.
[10] Munnemann K, Spiess H W. Nuclear magnetic resonance: The art of signal enhancement[J]. Nat Phys, 2011, 7(7): 522-523.
[11] Theis T, Ganssle P, Kervern G, et al. Parahydrogen-enhanced zero-field nuclear magnetic resonance[J]. Nat Phys, 2011, 7(7):571-575.
[12] Chen Y, Pang Y, Wu J, et al., Controlling the particle size of interpolymer complexes through host-guest interaction for drug delivery\[J\]. Langmuir, 2010, 26(11): 9 011-9 016.
[13] Jia Z, Zhang L, Chen Q, et al. Proton spin diffusion in polyethylene as a function of magic-angle spinning rate. A phenomenological approach[J]. J Phys Chem A, 2008, 112(6): 1 228-1 233.
[14] Wang X L, Tao F F, Sun P C, et al. Probing chain interpenetration in polymer glasses by H-1 dipolar filter solid-state NMR under fast magic angle spinning[J]. Macromolecules, 2007, 40(14): 4 736-4 739.
[15] Fu W G, Jiang R, Chen T H, et al. Evolution of interphase in styrene-butadiene block copolymers as revealed by 1H solid-state NMR: Effect of temperature and molecular architecture\[J\]. Polymer, 2010, 51(9): 2 069-2 076.
[16] Yao Y, Graf R, Spiess H, et al. Influence of crystal thickness and topological constraints on chain diffusion in linear polyethylene[J]. Macromol Rapid Commun, 2009, 30(13): 1 123-1 127.
[17] Zhang L, Liu Z, Chen Q, et al. Quantitative determination of phase content in multiphase polymers by combining spin-diffusion and CPMAS NMR[J]. Macromolecules, 2007, 40(15): 5 411-5 419.
[18] Ru G, Wang N, Huang S, et al. 1H HRMAS NMR study on phase transition of poly(N-isopropylacrylamide) gels with and without grafted comb-type chains[J]. Macromolecules, 2009, 42(6): 2 074-2 078.
[19] Gao X, Wang L, Luo H, et al. Crystalline phases in ethylene copolymers studied by solid-state NMR and DSC[J]. Macromolecules, 2010, 43(13): 5 713-5 722.
[20] Andrew E R, Bradbury A, Eades R G. Nuclear magnetic resonance spectra from a crystal rotated at high speed[J]. Nature, 1958, 182(4650): 1 659-1 659.
[21] Lowe I J. Free induction decays of rotating solids[J]. Phys Rev lett, 1959, 2(7): 285-287.
[22] Lesage A, Sakellariou D, Hediger S, et al. Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling[J]. J Magn Reson, 2003, 163(1): 105-113.
[23] Gerstein B C. High resolution NMR in randomly oriented solids with homonuclear dipolar broadening: Combined multiple pulse NMR and magic angle spinning[J]. J Chem Phys, 1977, 66(1): 361-362.
[24] Waugh J S, Huber L M, Haeberlen U. Approach to high-resolution NMR in solids[J]. Phys Rev Lett, 1968, 20(5): 180.
[25] Mansfield P. Symmetrized pulse sequences in high resolution NMR in solids[J]. J Phys A: Solid State Phys, 1971, 4(11): 1 444-1 452.
[26] Rhim W K, Elleman D D, Vaughan R W. Enhanced resolution for solid state NMR[J]. J Chem Phys, 1973, 58(4): 1 772-1 773.
[27] Burum D P, Rhim W K. Analysis of multiple pulse NMR in solids. III[J]. J Chem Phys, 1979, 71(2): 944-956.
[28] Hohwy M, Bower P V, Jakobsen H J, et al. A high-order and broadband CRAMPS experiment using z-rotational decoupling[J]. Chem Phys Lett, 1997, 273(5-6): 297-303.
[29] Hohwy M, Nielsen N C. Elimination of high order terms in multiple pulse nuclear magnetic resonance spectroscopy: Application to homonuclear decoupling in solids[J]. J Chem Phys, 1997, 106(18): 7 571-7 586.
[30] Bielecki A, Kolbert A C, Levitt M H. Frequency-switched pulse sequences: Homonuclear decoupling and dilute spin NMR in solids[J]. Chem Phys Lett, 1989, 155(4-5): 341-346.
[31] Bielecki A K A C, DeGroot H J M. Frequency-switched Lee-Goldburg sequence in solids\[J\]. Adv Magn Reson, 1990, (14): 111-124.
[32] Vinogradov E, Madhu P K, Vega S. High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment[J]. Chem Phys Lett, 1999, 314(5-6): 443-450.
[33] Vinogradov E, Madhu P K, Vega S. Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences[J]. Chem Phys Lett, 2002, 354(3-4): 193-202.
[34] Paul S, Schneider D, Madhu P K.1H Homonuclear dipolar decoupling using symmetry-based pulse sequences at ultra fast magicangle spinning frequencies[J]. J Magn Reson, 2010, 206(2): 241-245.
[35] Sakellariou D, Lesage A, Hodgkinson P, et al. Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation[J]. Chem Phys Lett, 2000, 319(3-4): 253-260.
[36] Elena B, de Pa-pe G, Emsley L. Direct spectral optimisation of proton-proton homonuclear dipolar decoupling in solid-state NMR[J]. Chem Phys Lett, 2004, 398(4-6): 532-538.
[37] Salager E, Stein R S, Steuernagel S, et al. Enhanced sensitivity in high-resolution 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultrafast MAS[J]. Chem Phys Lett, 2009, 469(4-6): 336-341.
[38] Gerstein B C, Pembleton R G, Wilson R C, et al. High resolution NMR in randomly oriented solids with homonuclear dipolar broadening: Combined multiple pulse NMR and magic angle spinning[J]. J Chem Phys, 1977, 66(1): 361-362.
[39] Taylor R E, Pembleton R G, Ryan L M, et al. Combined multiple pulse NMR and sample spinning: Recovery of 1H chemical shift tensors[J]. J Chem Phys, 1979, 71(11): 4 541-4 545.
[40] Hoult D I, Richards R E. Critical factors in the design of sensitive high resolution nuclear magnetic resonance spectrometers[J]. Proc R Soc London Ser A, 1975, 344(1638): 311-340.
[41] Ryan L M, Taylor R E, Paff A J, et al. An experimental study of resolution of proton chemical shifts in solids: Combined multiple pulse NMR and magic-angle spinning[J]. J Chem Phys, 1980, 72(1): 508-515.
[42] Madhu P K, Zhao X, Levitt M H. High-resolution 1H NMR in the solid state using symmetry-based pulse sequences[J]. Chem Phys Lett, 2001, 346(1-2): 142-148.
[43] Paul S, Thakur R S, Madhu P K. 1H homonuclear dipolar decoupling at high magic-angle spinning frequencies with rotor-synchronised symmetry sequences[J]. Chem Phys Lett, 2008, 456(4-6): 253-256.
[44] Amoureux J P, Hu B, Trébosc J. Enhanced resolution in proton solid-state NMR with very-fast MAS experiments[J]. J Magn Reson, 2008, 193(2): 305-307.
[45] Amoureux J P, Hu B, Trébosc J, et al. Homonuclear dipolar decoupling schemes for fast MAS[J]. Solid State Nucl Magn Reson, 2009, 35(1): 19-24.
[46] Gan Z H, Madhu P K, Amoureux J P, et al. A tunable homonuclear dipolar decoupling scheme for high-resolution proton NMR of solids from slow to fast magic-angle spinning[J]. Chem Phys Lett, 2011, 503(1-3): 167-170.
[47] Caravatti P, Neuenschwander P, Ernst R R. Characterization of heterogeneous polymer blends by two-dimensional proton spin diffusion spectroscopy[J]. Macromolecules, 1985, 18(1): 119-122.
[48] Caravatti P, Neuenschwander P, Ernst R R. Charcterization of polymer blends by selective proton spin-diffusion NMR measurements[J]. Macromolecules, 1986, 19(7): 1 889-1 895.
[49] Xu Lu(徐璐). Combined Solid-State NMR and Quantum Chemical Calculation Studies of Microstructure, Hydrogen Bond and Segmental Motion in Polymers(量化计算结合固体NMR研究高分子微观结构、氢键与链运动)[D]. Tianjin(天津):Nankai University(南开大学), 2010.
[50] Sommer W, Gottwald J, Demco D E, et al. Dipolar heteronuclear multiple-quantum NMR spectroscopy in rotating solids[J]. J Magn Reson Ser A, 1995, 113(1): 131-134.
[51] Saalw-chter K, Lange F, Matyjaszewski K, et al. BaBa-xy16: Robust and broadband homonuclear DQ recoupling for applications in rigid and soft solids up to the highest MAS frequencies[J]. J Magn Reson, 2011, 212(1): 204-215.
[52] Lee Y K, Kurur N D, Helmle M, et al. Efficient dipolar recoupling in the NMR of rotating solids. A sevenfold symmetric radiofrequency pulse sequence[J]. Chem Phys Lett, 1995, 242(3): 304-309.
[53] Hohwy M, Jakobsen H J, Eden M, et al. Broadband dipolar recoupling in the nuclear magnetic resonance of rotating solids: A compensated C7 pulse sequence[J]. J Chem Phys, 1998, 108(7): 2 686-2 694.
[54] Schmidt-Rohr K, Clauss J, Blümich B, et al. Miscibility of polymer blends investigated by 1H spin diffusion and 13C NMR detection[J]. Magn Reson Chem, 1990, 28(13): S3-S9.
[55] Egger N, Schmidt-Rohr K, Blümich B, et al. Solid state NMR investigation of cationic polymerized epoxy resins[J]. J Appl Polym Sci, 1992, 44(2): 289-295.
[56] Landfester K, Spiess H W. Characterization of interphases in core-shell latexes by solid-state NMR[J]. Acta Polym, 1998, 49(9): 451-464.
[57] Sun P C, Dang Q Q, Li B H, et al. Mobility, miscibility, and microdomain structure in nanostructured thermoset blends of epoxy resin and amphiphilic poly(ethylene oxide)-block-poly(propylene oxide)-block-poly(ethylene oxide) triblock copolymers characterized by solid-state NMR[J]. Macromolecules, 2005, 38(13): 5 654-5 667.
[58] Li X J, Fu W G, Wang Y N, et al. Solid-state NMR characterization of unsaturated polyester thermoset blends containing PEO-PPO-PEO block copolymers[J]. Polymer, 2008, 49(12): 2 886-2 897.
[59] Cai W Z, Schmidt-Rohr K, Egger N, et al. A solid-state n.m.r. study of microphase structure and segmental dynamics of poly(styrene-b-methylphenylsiloxane) diblock copolymers[J]. Polymer, 1993, 34(2): 267-276.
[60] Saalwachter K. Proton multiple-quantum NMR for the study of chain dynamics and structural constraints in polymeric soft materials[J]. Prog Nucl Magn Reson Spectrosc, 2007, 51(1): 1-35.
[61] Baum J, Pines A. NMR studies of clustering in solids[J]. J Am Chem Soc, 1986, 108(24): 7 447-7 454.
[62] Schneider M, Gasper L, Demco D E, et al. Residual dipolar couplings by 1H dipolar-encoded longitudinal magnetization, double- and triple-quantum nuclear magnetic resonance in cross-linked elastomers[J}. J Chem Phys, 1999, 111: 402-415.
[63] Fechete R, Demco D E, Blümich B. Enhanced sensitivity to residual dipolar couplings of elastomers by higher-order multiple-quantum NMR[J]. J Magn Reson, 2004, 169(1): 19-26.
[64] Saalwachter K. 1H multiple-quantum nuclear magnetic resonance investigations of molecular order in polymer networks. II. Intensity decay and restricted slow dynamics[J]. J Chem Phys, 2004, 120(1): 454-464.
[65] Saalwchter K, Klüppel M, Luo H, et al. Chain order in filled SBR elastomers: a proton multiple-quantum NMR study[J]. Appl Magn Reson, 2004, 27(3): 401-417.
[66] Chasse W, Valentin J L, Genesky G D, et al. Precise dipolar coupling constant distribution analysis in proton multiple-quantum NMR of elastomers[J]. J Chem Phys, 2011, 134(4): 044907.
[67] Saalw-chter K, Gottlieb M, Liu, et al. Gelation as studied by proton multiple-quantum NMR[J]. Macromolecules, 2007, 40(5): 1 555-1 561.
[68] Saalw-chter K. Detection of heterogeneities in dry and swollen polymer networks by proton low-field NMR spectroscopy[J]. J Am Chem Soc, 2003, 125(48): 14 684-14 685.
[69] Vaca C, aacute, vez F, et al. NMR Observation of entangled polymer dynamics: tube model predictions and constraint release[J]. Phys Rev lett, 2010, 104(19): 198305.
[70] Wang M, Bertmer M, Demco D E, et al. Indication of heterogeneity in chain-segment order of a PDMS layer grafted onto a silica surface by 1H multiple-quantum NMR[J]. Macromolecules, 2003, 36(12): 4 411-4 413.
[71] Li B, Xu L, Wu Q, et al. Various types of hydrogen bonds, their temperature dependence and water-polymer interaction in hydrated poly(acrylic acid) as revealed by H-1 solid-state NMR spectroscopy[J]. Macromolecules, 2007, 40(16): 5 776-5 786.
[72] Chevelkov V, Rehbein K, Diehl A, et al. Ultrahigh resolution in proton solid-state NMR spectroscopy at high levels of deuteration[J]. Angew Chem Int Edit, 2006, 45(23): 3 878-3 881.
[73] Wang X L, Gu Q, Sun Q, et al. Characterization of polymer compatibility by H-1 dipolar filter solid-state NMR under fast magic angle spinning[J]. Macromolecules, 2007, 40(25): 9 018-9 025.
[74] Gu Q, Wang X, Sun P, et al. Tracking the interdiffusion of polymers at a molecular level by 1H dipolar filter solid-state NMR under fast magic angle spinning[J]. Soft Matter, 2011, 7(2): 691-697.
[75] Liu Q H, Ma C, Hu B W, et al. Rotor-synchronized dipolar-filter sequence at fast MAS in solid-state NMR[J]. J Magn Reson, 2011, 212(2): 455-459.
[76] Brinkmann A, Levitt M H. Symmetry principles in the nuclear magnetic resonance of spinning solids: Heteronuclear recoupling by generalized Hartmann-Hahn sequences[J]. J Chem Phys, 2001, 115: 357-384.
[77] Brinkmann A, Edén M. Second order average Hamiltonian theory of symmetry-based pulse schemes in the nuclear magnetic resonance of rotating solids: Application to triple-quantum dipolar recoupling[J]. J Chem Phys, 2004, 120: 11 726-11 745.
[78] Campbell G C, VanderHart D L. Optimization of chemical-shift-based polarization gradients in 1H NMR spin-diffusion experiments on polymer blends with chemically similar constituents[J]. J Magn Reson, 1992, 96(1): 69-93.
[79] Cho G, Natansohn A. Investigation of phase structure of blends of poly\[(N-ethylcarbazol-3-yl)methyl methacrylate] and poly{2-[(3,5-Dinitrobenzoyl)oxy\]ethyl methacrylate} using 1H CRAMPS NMR[J]. Chem Mater, 1997, 9(1): 148-154.
[80] VanderHart D L, Prabhu V M, Lin E K. Proton NMR determination of miscibility in a bulk model photoresist system: Poly(4-hydroxystyrene) and the photoacid generator, Di(tert-butylphenyl)Iodonium perfluorooctanesulfonate[J]. Chem Mater, 2004, 16(16): 3 074-3 084.
[81] Fu Wei-gui(付维贵). Solid-State NMR Studies on the Microdomain Structure, Interactions and Dynamics of Typical Multiphase Polymer(典型多相聚合物中微相结构,相互作用及动力学的固体NMR研究)\[D\]. Tianjin(天津):Nankai University(南开大学), 2010.
[82] Schmidt-Rohr K, Mao J D. Selective dephasing of OH and NH proton magnetization based on 1H chemical-shift anisotropy recoupling[J]. J Magn Reson, 2002, 157(2): 210-217.
[83] Pines A, Gibby M G, Waugh J S. Proton-enhanced NMR of dilute spins in solids[J]. J Chem Phys, 1973, 59(2): 569-590.
[84] Christiansen S C, Hedin N, Epping J D, et al. Sensitivity considerations in polarization transfer and filtering using dipole-dipole couplings: Implications for biomineral systems[J]. Solid State Nucl Magn Reson, 2006, 29(1-3): 170-182.
[85] Peng W K, Takeda K. Efficient cross polarization with simultaneous adiabatic frequency sweep on the source and target channels[J]. J Magn Reson, 2007, 188(2): 267-274.
[86] Weingarth M, Bodenhausen G, Tekely P. Low-power decoupling at high spinning frequencies in high static fields[J]. J Magn Reson, 2009, 199(2): 238-241.
[87] Hou G, Ding S, Zhang L, et al. Breaking the T1 constraint for quantitative measurement in magic angle spinning solid-state NMR spectroscopy[J]. J Am Chem Soc, 2010, 132(16): 5 538-5 539.
[88] deAzevedo E R, Hu W G, Bonagamba T J, et al. Centerband-only detection of exchange: Efficient analysis of dynamics in solids by NMR[J]. J Am Chem Soc, 1999, 121(36): 8 411-8 412.
[89] Lesage A, Bardet M, Emsley L. Through-bond carbon-carbon connectivities in disordered solids by NMR[J]. J Am Chem Soc, 1999, 121(47): 10 987-10 993.
[90] deAzevedo E R, Hu W G, Bonagamba T J, et al. Principles of centerband-only detection of exchange in solid-state nuclear magnetic resonance, and extension to four-time centerband-only detection of exchange[J]. J Chem Phys, 2000, 112(20): 8 988-9 001.
[91] Lesage A, Charmont P, Steuernagel S, et al. Complete resonance assignment of a natural abundance solid peptide by through-bond heteronuclear correlation solid-state NMR[J]. J Am Chem Soc, 2000, 122(40): 9 739-9 744.
[92] Krushelnitsky A, deAzevedo E, Linser R, et al. Direct observation of millisecond to second motions in proteins by dipolar CODEX NMR spectroscopy[J]. J Am Chem Soc, 2009, 131(34): 12 097-12 099.
[93] Bennett A E, Rienstra C M, Auger M, et al. Heteronuclear decoupling in rotating solids[J]. J Chem Phys, 1995, 103(16): 6 951-6 958.
[94] Gan Z, Ernst R R. Frequency- and phasemodulated heteronuclear decoupling in rotating solids[J]. Solid State Nucl Magn Reson, 1997, 8(3): 153-159.
[95] Takegoshi K, Mizokami J, Terao T. 1H decoupling with third averaging in solid NMR[J]. Chem Phys Lett, 2001, 341(5-6): 540-544.
[96] Fung B M, Khitrin A K, Ermolaev K. An improved broadband decoupling sequence for liquid crystals and solids[J]. J Magn Reson, 2000, 142(1): 97-101.
[97] Detken A, Hardy E H, Ernst M, et al. Simple and efficient decoupling in magic-angle spinning solid-state NMR: the XiX scheme[J]. Chem Phys Lett, 2002, 356(3-4): 298-304.
[98] De Pa-pe G, Sakellariou D, Hodgkinson P, et al. Heteronuclear decoupling in NMR of liquid crystals using continuous phase modulation[J]. Chem Phys Lett, 2003, 368(5-6): 511-522.
[99] De Pa-pe G, Hodgkinson P, Emsley L. Improved heteronuclear decoupling schemes for solid-state magic angle spinning NMR by direct spectral optimization[J]. Chem Phys Lett, 2003, 376(3-4): 259-267.
[100] Chandran C V, Br-uniger T. Efficient heteronuclear dipolar decoupling in solid-state NMR using frequency-swept SPINAL sequences[J]. J Magn Reson, 2009, 200(2): 226-232.
[101] Thakur R S, Kurur N D, Madhu P K. Swept-frequency two-pulse phase modulation for heteronuclear dipolar decoupling in solid-state NMR[J]. Chem Phys Lett, 2006, 426(4-6): 459-463.
[102] Vinod Chandran C, Madhu P K, Kurur N D, et al. Swept-frequency two-pulse phase modulation (SWf-TPPM) sequences with linear sweep profile for heteronuclear decoupling in solid-state NMR\[J\]. Magn Reson Chem, 2008, 46(10): 943-947.
[103] Weingarth M, Tekely P, Bodenhausen G. Efficient heteronuclear decoupling by quenching rotary resonance in solid-state NMR[J]. Chem Phys Lett, 2008, 466(4-6): 247-251.
[104] Paul S, Mithu V S, Kurur N D, et al. Efficient heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance at rotary resonance conditions[J]. J Magn Reson, 2010, 203(1): 199-202.
[105] Paul S, Kurur N D, Madhu P K. On the choice of heteronuclear dipolar decoupling scheme in solid-state NMR[J]. J Magn Reson, 2010, 207(1): 140-148.
[106] Zhang S, Wu X, Zhang H, et al. Quantitative measurement of rare spins in solid state cross polarization NMR[J]. Chem Phys Lett, 1990, 165(6): 465-468.
[107] Fu R, Hu J, Cross T A. Towards quantitative measurements in solid-state CPMAS NMR: A Lee-Goldburg frequency modulated crosspolarization scheme[J]. J Magn Reson, 2004, 168(1): 8-17.
[108] Shu J, Chen Q, Zhang S. Quantification of cross polarization with relaxation compensated reciprocity relation in NMR[J]. Chem Phys Lett, 2008, 462(1-3): 125-128.
[109] Shu J, Li P, Chen Q, et al. Quantitative measurement of polymer compositions by NMR spectroscopy: Targeting polymers with marked difference in phase mobility[J]. Macromolecules, 2010, 43(21): 8 993-8 996.
[110] Takegoshi K, Nakamura S, Terao T. 13C-13C polarization transfer by resonant interference recoupling under magic-angle spinning in solid-state NMR[J]. Chem Phys Lett, 1999, 307(5-6): 295-302.
[111] Takegoshi K, Nakamura S, Terao T. 13C-1H dipolar-assisted rotational resonance in magic-angle spinning NMR[J]. Chem Phys Lett, 2001, 344(5-6): 631-637.
[112] Takegoshi K, Nakamura S, Terao T. 13C-1H dipolar-driven 13C-13C recoupling without 13C rf irradiation in nuclear magnetic resonance of rotating solids[J]. J Chem Phys, 2003, 118(5): 2 325-2 341.
[113] Schmidt-Rohr K, Clauss J, Spiess H W. Correlation of structure, mobility, and morphological information in heterogeneous polymer materials by two-dimensional wideline-separation NMR spectroscopy\[J\]. Macromolecules, 1992, 25(12): 3 273-3 277.
[114] Tekely P, Palmas P, Mutzenhardt P. Elimination of heteronuclear dipolar interactions from carbon-13-detected proton spectra in wideline-separation nuclear magnetic resonance spectroscopy[J]. Macromolecules, 1993, 26(26): 7 363-7 365.
[115] van Rossum B J, de Groot, Ladizhansky C P, et al. A method for measuring heteronuclear (1H-13C) distances in high speed MAS NMR[J]. J Am Chem Soc, 2000, 122(14): 3 465-3 472.
[116] Hong M, Yao X, Jakes K, et al. Investigation of molecular motions by lee-goldburg cross-polarization NMR spectroscopy[J]. J Phys Chem B, 2002, 106(29): 7 355-7 364.
[117] Hartmann S R, Hahn E L. Nuclear double resonance in the rotating frame[J]. Phys Rev, 1962, 128(5): 2042.
[118] Qiu X, Mirau P A. WIM/WISE NMR studies of chain dynamics in solid polymers and blends[J]. J Magn Reson, 2000, 142(1): 183-189.
[119] Hediger S, Lesage A, Emsley L. A new NMR method for the study of local mobility in solids and application to hydration of biopolymers in plant cell walls[J]. Macromolecules, 2002, 35(13): 5 078-5 084.
[120] Mulder F M, Jansen B J P, Lemstra P J, et al. Pronounced poly(methyl methacrylate) dynamics induced by blending morphology[J]. Macromolecules, 2000, 33(2): 457-460.
[121] Ohgo K, Niemczura W P, Muroi T, et al. Wideline separation (WISE) NMR of native elastin[J]. Macromolecules, 2009, 42(22): 8 899-8 906.
[122] Caravatti P, Bodenhausen G, Ernst R R. Heteronuclear solid-state correlation spectroscopy[J]. Chem Phys Lett, 1982, 89(5): 363-367.
[123] Caravatti P, Braunschweiler L,Ernst R R. Heteronuclear correlation spectroscopy in rotating solids[J]. Chem Phys Lett, 1983, 100(4): 305-310.
[124] Bielecki A, Burum D P, Rice D M, et al. Solid-state two-dimensional carbon-13-proton correlation (HETCOR) NMR spectrum of amorphous poly(2,6-dimethyl-p-phenylene oxide) (PPO)[J]. Macromolecules, 1991, 24(17): 4 820-4 822.
[125] Jia X, Wolak J, Wang X, et al. Independent calibration of 1H spin-diffusion coefficients in amorphous polymers by intramolecular polarization transfer[J]. Macromolecules, 2003, 36(3): 712-718.
[126] Hou S S, Beyer F L, Schmidt-Rohr K. Highsensitivity multinuclear NMR spectroscopy of a smectite clay and of clay-intercalated polymer[J]. Solid State Nucl Magn Reson, 2002, 22(2-3): 110-127.
[127] Jia X, Wang X, Tonelli A E, et al. Two-dimensional spin-diffusion NMR reveals differential mixing in biodegradable polymer blends[J]. Macromolecules, 2005, 38(7): 2 775-2 780.
[128] Lesage A, Sakellariou D, Steuernagel S, et al. Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiplequantum spectroscopy[J]. J Am Chem Soc, 1998, 120(50): 13 194-13 201.
[129] Lesage A, Emsley L. Through-bond heteronuclear single-quantum correlation spectroscopy in solid-state NMR, and comparison to other through-bond and through-space experiments[J]. J Magn Reson, 2001, 148(2): 449-454.
[130] Lesage A, Auger C, Caldarelli S, et al. Determination of through-bond carbon-carbon connectivities in solid-state NMR using the INADEQUATE experiment[J]. J Am Chem Soc, 1997, 119(33): 7 867-7 868.
[131] Wu C H, Ramamoorthy A, Opella S J. High-resolution heteronuclear dipolar solid-state NMR spectroscopy[J]. J Magn Reson Ser A, 1994, 109(2): 270-272.
[132] Hester R K, Ackerman J L, Neff B L, et al. Separated local field spectra in NMR: Determination of structure of solids[J]. Phys Rev lett, 1976, 36(18): 1 081-1 083.
[133] A. Ramamoorthy Y W, Dong-Kuk Lee. PISEMA solid-state NMR spectroscopy[J]. Annu Rep NMR Spectrosc, 2004, 52: 1-52.
[134] Olve B, Peersen X W, Irina Kustanovich, et al. Variable -amplitude cross-polarization MAS NMR[J]. J Magn Reson A, 1993, 104(3): 334-339.
[135] Lee M, Goldburg W I. Nuclear-magnetic-resonance line narrowing by a rotating rf field[J]. Phys Rev, 1965, 140(4A): A1261-A1271.
[136] Yamamoto K, Lee D K, Ramamoorthy A. Broadband-PISEMA solid-state NMR spectroscopy[J]. Chem Phys Lett, 2005, 407(4-6): 289-293.
[137] Lee D K, Narasimhaswamy T, Ramamoorthy A. PITANSEMA, a low-power PISEMA solid-state NMR experiment[J]. Chem Phys Lett, 2004, 399(4-6): 359-362.
[138] Nevzorov A A, Opella S J. A “Magic Sandwich” pulse sequence with reduced offset dependence for high-resolution separated local field spectroscopy[J]. J Magn Reson, 2003, 164(1): 182-186.
[139] Nevzorov A A, Opella S J. Selective averaging for high-resolution solid-state NMR spectroscopy of aligned samples[J]. J Magn Reson, 2007, 185(1): 59-70.
[140] Ramamoorthy A, Opella S J. Two-dimensional chemical shift/heteronuclear dipolar coupling spectra obtained with polarization inversion spin exchange at the magic angle and magic-angle sample spinning (PISEMAMAS)[J]. Solid State Nucl Magn Reson, 1995, 4(6): 387-392.
[141] Dvinskikh S V, Zimmermann H, Maliniak A, et al. Heteronuclear dipolar recoupling in liquid crystals and solids by PISEMA-type pulse sequences[J]. J Magn Reson, 2003, 164(1): 165-170.
[142] Dvinskikh S V, Sandstr-m D. Frequency offset refocused PISEMA-type sequences[J]. J Magn Reson, 2005, 175(1): 163-169.
[143] Zhang R C, He X, Fu W G, et al. Efficient identification of different types of carbons in organic solids by 2D solid-state NMR spectroscopy[J]. J Phys Chem A, 2011, 115(42): 11 665-11 670.
[144] Hartzell C J, Whitfield M, Oas T, et al. Determination of the nitrogen-15 and carbon-13 chemical shift tensors of L-[13C]alanyl-L-[15N]alanine from the dipole-coupled powder patterns[J]. J Am Chem Soc, 1987, 109(20): 5 966-5 969.
[145] de Dios A C, Oldfield E. Evaluating 19F chemical shielding in fluorobenzenes: Implications for chemical shifts in proteins[J]. J Am Chem Soc, 1994, 116(16): 7 453-7 454.
[146] Heller J, Laws D D, Tomaselli M, et al. Determination of dihedral angles in peptides through experimental and theoretical studies of αCarbon chemical shielding tensors[J]. J Am Chem Soc, 1997, 119(33): 7 827-7 831.
[147] Hu J Z, Solum M S, Taylor C M V, et al. Structural determination in carbonaceous solids using advanced solid state NMR techniques\[J\]. Energy & Fuels, 2000, 15(1): 14-22.
[148] Duncan T. A compilation of chemical shift anisotropies[M]. Chicago: Farragut Press edition, 1990.
[149] Herzfeld J, Berger A E. Sideband intensities in NMR spectra of samples spinning at the magic angle[J]. J Chem Phys, 1980, 73: 6 021-6 030.
[150] Liu S F, Mao J D, Schmidt-Rohr K. A robust technique for two-dimensional separation of undistorted chemical-shift anisotropy powder patterns in magic-angle-spinning NMR[J]. J Magn Reson, 2002, 155(1): 15-28.
[151] Tycko R, Dabbagh G, Mirau P A. Determination of chemical-shift-anisotropy Lineshapes in a two-dimensional magic-angle-spinning NMR experiment[J]. J Magn Reson, 1989, 85(2): 265-274.
[152] Bax A, Szeverenyi N M, Maciel G E. Chemical shift anisotropy in powdered solids studied by 2D FT NMR with flipping of the spinning axis[J]. J Magn Reson, 1983, 55(3): 494-497.
[153] Bax A, Szeverenyi N M, Maciel G E. Chemical shift anisotropy in powdered solids studied by 2D FT CP/MAS NMR[J]. J Magn Reson, 1983, 51(3): 400-408.
[154] Terao T, Fujii T, Onodera T, et al. Switching-angle sample-spinning NMR spectroscopy for obtaining powder-pattern-resolved 2D spectra: Measurements of 13C chemical-shift anisotropies in powdered 3,4-dimethoxybenzaldehyde[J]. Chem Phys Lett, 1984, 107(2): 145-148.
[155] Ishii Y, Terao T. Manipulation of nuclear spin Hamiltonians by rf-field modulations and its applications to observation of powder patterns under magic-angle spinning\[J\]. J Chem Phys, 1998, 109: 1 366-1 374.
[156] Hong M, Yao X. Homonuclear decoupled 13C chemical shift anisotropy in 13C doubly labeled peptides by selective-pulse solid-state NMR[J]. J Magn Reson, 2003, 160(2): 114-119.
[157] Xu Lu(徐璐), Li Bao-hui(李宝会), Sun Ping-chuan(孙平川). Chemical shift anisotropy of polypropylenes: Theoretical calculation and experimental results from solid-state NMR experiments(高分子化学位移的量化计算与固体NMR实验研究)[J]. Chinese J Magn Reson(波谱学杂志), 2010, 27(4): 597-608.
[158] Yang Y, Schuster M, Blümich B, et al. Dynamic magic-angle spinning nmr spectroscopy: Exchange-induced sidebands[J]. Chem Phys Lett, 1987, 139(3-4): 239-243.
[159] Yang Y, Hagemeyer A, Blümich B, et al. 2D magic angle spinning NMR spectroscopy: Correlation between molecular order and dynamics[J]. Chem Phys Lett, 1988, 150(1-2): 1-5.
[160] Yang Y, Hagemeyer A, Spiess H W. An order-exchange-correlated two-dimensional NMR study of slow molecular motion in highly oriented crystalline poly(oxymethylene)[J]. Macromolecules, 1989, 22(2): 1 004-1 006.
[161] deAzevedo E R, Bonagamba T J, Reichert D. Molecular dynamics in solid polymers[J]. Prog Nucl Magn Reson Spectrosc, 2005, 47(3-4): 137-164.
[162] Pascui O, Beiner M, Reichert D. Identification of slow dynamic processes in poly(n-hexyl Methacrylate) by solid-state 1D-MAS exchange NMR[J]. Macromolecules, 2003, 36(11): 3 992-4 003.
[163] deAzevedo E R, Bonagamba T J, Schmidt-Rohr K. Pure-exchange solid-state NMR[J]. J Magn Reson, 2000, 142(1): 86-96.
[164] deAzevedo E R, Tozoni J R, Schmidt-Rohr K, et al. Analysis of one-dimensional pure-exchange NMR experiments for studying dynamics with broad distributions of correlation times[J]. J Chem Phys, 2005, 122: 154506.
[165] Gérardy-Montouillout V, Malveau C, Tekely P, et al. ODESSA, a New 1D NMR exchange experiment for chemically equivalent nuclei in rotating solids[J]. J Magn Reson Ser A, 1996, 123(1): 7-15.
[166] Reichert D, Zimmermann H, Tekely P, et al. Time-reverse ODESSA. A 1D exchange experiment for rotating solids with several groups of equivalent nuclei[J]. J Magn Reson, 1997, 125(2): 245-258.
[167] Luz Z, Tekely P, Reichert D. Slow exchange involving equivalent sites in solids by one-dimensional MAS NMR techniques[J]. Prog Nucl Magn Reson Spectrosc, 2002, 41(1-2): 83-113.
[168] Wolak J E, White J L. Factors That Allow Polyolefins To Form Miscible Blends: Polyisobutylene and Head-to-Head Polypropylene[J]. Macromolecules, 2005, 38(25): 10 466-10 471.
[169] Wachowicz M, Gill L, Wolak J, et al. Print-polypropylene and polyethylene-copolymer blend miscibility: slow chain dynamics in individual blend components near the glass transition[J]. Macromolecules, 2008, 41(8): 2 832-2 838.
[170] Wachowicz M, Gill L, White J L. Polyolefin blend miscibility: Polarization transfer versus direct excitation exchange NMR[J]. Macromolecules, 2008, 42(2): 553-555.
[171] Saalwachter K, Schmidt-Rohr K. Relaxation-induced dipolar exchange with recoupling-An MAS NMR method for determining heteronuclear distances without irradiating the second spin[J]. J Magn Reson, 2000, 145(2): 161-172. |