波谱学杂志

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一种提高核磁共振快弛豫信号测量精度的方法

马莹颖,张宫*,廖中枢   

  1. 长江大学油气资源与勘探技术教育部重点实验室
  • 收稿日期:2023-09-12 修回日期:2023-10-09 出版日期:2023-10-10 在线发表日期:2023-10-10
  • 通讯作者: 张宫 E-mail:zhanggong@yangtzeu.edu.cn

A Method for Improving the Measurement Accuracy of Nuclear Magnetic Resonance Fast Relaxation Signal

MA Yingying, ZHANG Gong*, LIAO Zhongshu   

  1. Key Laboratory of Exploration Technologies for Oil and Gas Resources of Education Ministry, Yangtze University, Wuhan 430100, China
  • Received:2023-09-12 Revised:2023-10-09 Published:2023-10-10 Online:2023-10-10
  • Contact: ZHANG Gong E-mail:zhanggong@yangtzeu.edu.cn

摘要: 核磁共振技术能够直接探测样品中水、烃等含氢流体信号并对其含量及所处环境进行定量表征,广泛应用在油气勘探领域.在对页岩油气、致密油气等含有大量超短弛豫组分样品进行测量时,由于CPMG脉冲序列观测到的前端信号数据量过少导致测量信号不稳定,快弛豫组分结果可靠性较低.提出了多次微变回波间隔测量(MCTEM)的方法,在测量阶段加密了对核磁共振前端信号数据的采集,反演阶段采用了多次测量回波数据的联合反演,可以得到更加精确的短弛豫T2谱.通过数值模拟和岩心物理实验对MCTEM方法进行了验证,结果显示MCTEM方法能够改善由回波间隔TE偏高引起的T2谱短弛豫组分峰消失的问题,可以有效提高短弛豫信号的测量精度.

关键词: 核磁共振, 测量精度, 多次微变回波间隔测量方法, 快速弛豫组分

Abstract: Nuclear magnetic resonance (NMR) technology can detect hydrogen signals in the hydrogen-containing fluids, such as water and hydrocarbon, directly. It can provide quantitative characterization of the fluid content and surrounding environment, thus finds extensive application in oil and gas exploration field. However, when measuring samples contain ultra-short relaxation components, such as shale oil and gas, the reliability of measurement results tends to be very low because only a small number of front-end signals in CPMG pulse sequence can be obtained for the fast relaxation components. Thus, a multiple micro echo interval measurement (MCTEM) method was proposed in this research. In the measurement stage, the proposed method acquired more NMR front-end signals. In the inversion stage, multiple echo data were adopted for the joint inversion. It contributed to forming an accurate short relaxation T2 spectrum. MCTEM method was validated through numerical simulations and rock physics experiments. It was concluded from the results that MCTEM method could improve the problem of peak disappearance for short relaxation components in T2 spectrum caused by high echo interval. MCTEM method could enhance the measurement accuracy of short relaxation signals effectively.

Key words: NMR, Measurement accuracy, Multiple micro echo interval measurement, Fast relaxation components

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