Chinese Journal of Magnetic Resonance ›› 2021, Vol. 38 ›› Issue (4): 533-542.doi: 10.11938/cjmr20212936

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Solid-State NMR Studies on the Surface Structure and Properties of Oxide Nanomaterials

Xi-feng XIA1,Wen-jing ZHANG2,Zhi-ye LIN2,Xiao-kang KE2,Yu-jie WEN2,Fang WANG2,Jun-chao CHEN2,*(),Lu-ming PENG2,*()   

  1. 1. Analysis and Testing Center, Nanjing University of Science and Technology, Nanjing 210094, China
    2. Key Laboratory of Mesoscopic Chemistry of Ministry of Education and Collaborative Innovation Center of Chemistry for Life Sciences, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210023, China
  • Received:2021-07-13 Online:2021-12-05 Published:2021-08-18
  • Contact: Jun-chao CHEN,Lu-ming PENG E-mail:cjcnuaa@163.com;luming@nju.edu.cn

Abstract:

Many applications of oxide nanomaterials depend on their surface structure and properties. Solid-state nuclear magnetic resonance (NMR) spectroscopy has been used to obtain such key information in related studies. This paper summarizes two recently developed approaches based on solid-state NMR spectroscopy for determining the surface structure and properties of oxide nanomaterials, including surface-selective isotopic labeling 17O NMR and dynamic nuclear polarization surface enhanced NMR spectroscopy. The development trend for investigating oxide nanomaterials with solid-state NMR spectroscopy is also introduced.

Key words: oxide nanomaterials, surface structure and properties, 17O, solid-state nuclear magnetic resonance spectroscopy, dynamic nuclear polarization

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