Chinese Journal of Magnetic Resonance ›› 2008, Vol. 25 ›› Issue (3): 408-414.

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Synthesis and Structure Elucidation of New Spiro Compounds with Polyfluoroalkyl Group

SHI Zhi-jian1,2*; ZHAO Yang1; CAO Wei-guo1,2; ZHANG Shun-li1; LIU Mei1, DENG Hong-mei3   

  1. (1.Department of Chemistry, Shanghai University, Shanghai 200444, China; 2.Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032, China; 3.The Center for Tesing, Shanghai University, Shanghai 200444, China)
  • Received:2007-09-07 Revised:2007-12-12 Online:2008-09-05 Published:2009-12-05
  • Contact: SHI Zhi-jian

Abstract: A spiro compound with polyfluoroalkyl group was synthesized. Its structure was elucidated by 1H NMR, 13C NMR, IR, MS, 2D NMR and X-diffraction. The spectral features and the space structure of the compound were also discussed.

Key words: polyfluoroalkylated, spiro compound, structure, X-diffraction

CLC Number: