双重低通滤波的HMBC实验

波谱学杂志 ›› 1996, Vol. 13 ›› Issue (3): 253-257.

双重低通滤波的HMBC实验

孔祥铭¹, 黄永仁²

1. 上海石油化工研究院, 上海 201208;
2. 上海华东师范大学分析测试中心, 上海 200062

收稿日期:1995-09-04 修回日期:1995-11-12 出版日期:1996-06-05 发布日期:2018-01-17
基金资助:
国家自然科学基金和国家教委博士点基金资助项目

HMBC EXPERIMENT WITH DOUBLE LOW-PASS J-FILTERS

Kong Xiangming¹, Huang Yongren²

1. Shanghai Research institute of Petrochemical Technology, Shanghai 201208;
2. Analytical Center, East China Normal University, Shanghai 200062

Received:1995-09-04 Revised:1995-11-12 Online:1996-06-05 Published:2018-01-17

摘要/Abstract

摘要： 利用两个低通滤波器,在反转检测的异核远程相关实验(HMBC)中消除由直接相关引起的卫星峰.消除其对远程相关峰的干扰,不仅理论上说明了其原理,而且在实验上得到证实.同时此实验不会引起灵敏度的下降.

关键词: 低通滤波器, HMBC实验

Abstract: Two low-pass J-filters are introduced into HMBC experiment to suppress all direct J-coupling peaks and do away with the interference of direct J-coupling peaks and long range J-upling peaks which may occur in HMBC spectra of some molecules. Theoretical analysis and experiments show that the purpose of suppressing all direct J-coupling peaks can be achieved with almost no loss of intensity of long range J-coupling peaks.

Key words: Low-pass, J-filter, HMBC experiment

孔祥铭, 黄永仁. 双重低通滤波的HMBC实验[J]. 波谱学杂志, 1996, 13(3): 253-257.

Kong Xiangming, Huang Yongren. HMBC EXPERIMENT WITH DOUBLE LOW-PASS J-FILTERS[J]. Chinese Journal of Magnetic Resonance, 1996, 13(3): 253-257.

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