波谱学杂志 ›› 2001, Vol. 18 ›› Issue (3): 263-267.

• 研究论文 • 上一篇    下一篇

新型萘酰亚胺衍生物的13C NMR研究

贺彩霞1,王复1,史新梅1,潘铁英1,甘家安2,陈孔常2,田禾2   

  1. 1.华东理工大学分析测试中心,上海 200237;2.华东理工大学精细化工研究所,上海 200237
  • 收稿日期:2001-04-23 修回日期:2001-05-24 出版日期:2001-09-05 发布日期:2001-09-05
  • 作者简介:贺彩霞(1970-),女,博士.
  • 基金资助:

    国家自然科学基金资助项目(29836150).

13C NMR STUDY OF NAPHTHALIMIDE DERIVATIVES

HE Cai-xia1, WANG Fu1, SHI Xin-mei1, PAN Tie-ying1, GAN Jia-an2,  CHEN Kong-chang2, TIAN He2   

  1. 1.Analysis and Research Center, East China University of Science and Technology,  Shanghai 200237; 2.Institute of Fine Chemicals, East China University of Science and Technology,  Shanghai 200237
  • Received:2001-04-23 Revised:2001-05-24 Online:2001-09-05 Published:2001-09-05
  • Supported by:

    国家自然科学基金资助项目(29836150).

摘要:

报道了四种新的萘酰亚胺衍生物的13C NMR谱. 应用1H、13C、DEPT、HMQC、HMBC 等谱确定了这四种化合物的分子结构,并对全部谱峰进行了归属,探讨了分子结构对13C NMR化学位移的影响.

关键词: 萘酰亚胺, 13C NMR, 化学位移 

Abstract:

Naphthalimides  are important organic compounds used in the field of biolog y ,chemistry, medicine, etc. In this paper, the 13C NMR data of 4 new naphthal imides are reported and their structures were determined by 1H,  1H- 1H COSY, HMQC and HMBC methods. The 13C chemical shifts of all of the 4 compounds  ha ve been assigned. The factors influencing the chemical shifts are discussed.

Key words: Naphthalimides,  13C NMR, Chemical shifts

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