波谱学杂志

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2D NMR在泥页岩物性及流体评价中的应用探讨

牛强1,2,王志战3,曾溅辉1,王鑫2,杜焕福2,盖姗姗2*   

  1. 1. 中国石油大学(北京) 地球科学学院,北京 102249;2. 中石化胜利石油工程有限公司 地质录井公司, 山东 东营 257064;3. 中国石化石油工程技术研究院 测录井研究所,北京 100101
  • 收稿日期:2013-07-04 修回日期:2013-11-05 出版日期:2014-06-05 发布日期:2014-06-05
  • 作者简介:牛强(1975-),男,山东东营人,高级工程师,博士研究生,目前主要从事非常规油气层评价技术研究. *通讯联系人,盖姗姗,电话:13589958586,E-mail: slniuq@126.com.

Evaluating Shale Porosity and Oil Content with 2D NMR

 NIU Qiang1,2,WANG Zhi-zhan3,ZENG Jian-hui1,WANG Xin2,DU Huan-fu2,GAI Shan-shan2*


 
  

  1. 1. College of Earth Science, China University of Petroleum (Beijing), Beijing 102249, China; 2. Geologging Company of Sheng-li Petroleum Engineering Company Limited, SINOPEC, Dongying 257064, China; 3. SINOPEC Research Institute of Petroleum Engineering, Beijing 100101, China
  • Received:2013-07-04 Revised:2013-11-05 Online:2014-06-05 Published:2014-06-05
  • About author:*Corresponding author:GAI Shan-shan, Tel:13589958586,E-mail: slniuq@126.com.

摘要:

纳米级孔隙、非达西渗流、自生自储是泥页岩油气层的主要特征,常规NMR技术难以检测到T2弛豫时间短于0.1 ms的纳米级孔隙,并难以准确评价泥页岩储层中的孔隙流体性质与含量.为了解决以上问题,以济阳坳陷下第三系沙河街组泥页岩油气主要勘探层段为研究对象,采用高分辨率2D NMR技术对采自3口井的11块泥页岩样品分别进行1D、2D NMR分析.结果表明,T2谱能够检测到泥页岩中的全部孔隙量;D-T2谱能够准确评价孔隙流体类型与含量,且核磁含油饱和度与石油的产液量、岩石热解的液态烃量具有可对比性.该项研究对精细评价泥页岩油气储层具有十分重要的意义,对进一步发展高分辨率2D NMR技术具有一定的促进作用.

关键词: 低场核磁共振(low-field NMR), 二维磁共振(2D NMR), 泥页岩, 纳米级孔隙, 流体类型和含量

Abstract:

Compared with conventional reservoir, shale reservoir is characterized by nanoscale pores, non-Darcy flow and self-generating/self-preserving properties. However, it is difficult to probe components in nanoscale pores with T2 relaxation time less than 0.1 ms, and to evaluate fluid types and content in shale reservoir with conventional NMR technology. In this study, high resolution 2D NMR technology was adopted to evaluate eleven shale samples collected from three wells in Shahejie formation of Jiyang Depression. By comparing with the data from formation testing and rock pyrolysis, it was confirmed that the T2spectrum measured with 2D NMR could reflect the properties of nanoscale pores, and D-T2 spectrum could be used to evaluate fluid types and content. The work suggested that high resolution 2D NMR technology is useful in unconventional resource exploration of shale.

Key words: low-field NMR, 2D NMR, shale, nano-scale pore, fluid types and content

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