变角二维谱实验

波谱学杂志 ›› 1990, Vol. 7 ›› Issue (3): 313-319.

变角二维谱实验

傅日强, 叶朝辉

中国科学院武汉物理所波谱与原子分子物理开放研究实验室

收稿日期:1989-10-09 修回日期:1989-11-16 出版日期:1990-09-05 发布日期:2018-01-23
基金资助:
国家自然科学基金

2D FLIPPING ANGLE EXPERIMENT

Fu Riqiang, Ye Chaohui

Laboratory of Magnetic Resonance and Atomic and Molecular Physics, Wuhan Institute of Physics, Academia Sinica, Wuhan, China

Received:1989-10-09 Revised:1989-11-16 Online:1990-09-05 Published:2018-01-23

摘要/Abstract

摘要： 本文描述了用同步驱动控制电路的变角机构,在Bruker WP-80谱仪上实现固体变角方法的二维谱实验。应用该变角机构,获得了固体粉末的化学位移各向同性和各向异性的二维分解谱。

关键词: 同步驱动控制电路, 变角实验, 固体二维核磁共振

Abstract: A synchronous driving and controlling circuit is described in this paper. 2D chemical shift isotropy and anisotropy correlation spectra of powdered soilds have been obtained with this flipping angle device attached to a Bruker WP-80 NMR spectrometer.

Key words: Synchronous driving and controlling circuit, Flipping angle experiment, 2D NMR spectroscopy of solids

傅日强, 叶朝辉. 变角二维谱实验[J]. 波谱学杂志, 1990, 7(3): 313-319.

Fu Riqiang, Ye Chaohui. 2D FLIPPING ANGLE EXPERIMENT[J]. Chinese Journal of Magnetic Resonance, 1990, 7(3): 313-319.