固体核磁共振样品制备系统的自主研制

陈阳,周萌,李勇,杨海军

Independent Development of Sample Preparation Tools for Solid-state NMR

CHEN Yang,ZHOU Meng,LI Yong,YANG Haijun

图8 自制转子的27Al SSNMR谱图，仪器型号为JNM-ECZ600R，探头为3.2 mm探头，转速为12 kHz，累加次数为128次

Fig. 8 The 27Al SSNMR spectrum of the self-made rotor performed on a JEOL JNM-ECZ600R NMR spectrometer. A 3.2 mm probe was used with a spinning rate of 12 kHz using 128 scans