固-液-气三相环境下非均相苯加氢反应的原位核磁共振研究
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随松,高国梁,王雪璐*( ),魏达秀*( ),姚叶锋*( )
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An Operando Nuclear Magnetic Resonance Study on Solid-Liquid-Gas Heterogeneous Benzene Hydrogenation Reaction
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Song SUI,Guo-liang GAO,Xue-lu WANG*( ),Da-xiu WEI*( ),Ye-feng YAO*( )
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图5. (a) 1, 3-环己二烯加氢过程;(b)不同反应时间采集的1H NMR谱.实验温度为298 K,压力为2.5 bar
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Fig.5. (a) Hydrogenation of 1, 3-cyclohexadiene; (b)1H NMR spectra of 1, 3-cyclohexadiene hydrogenation reaction, acquired at different reaction time. The experimental temperature is 298 K and the pressure is 2.5 bar
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