Chinese Journal of Magnetic Resonance ›› 2017, Vol. 34 ›› Issue (3): 357-364.doi: 10.11938/cjmr20162517

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Microwave Bridge in a DNP-EPR Multifunctional Spectrometer:Design and Implementation

LIU Zao1,2, ZHU Tian-xiong1, HE Yu-gui1, CHEN Jun-fei1,2, FENG Ji-wen1, LIU Chao-yang1   

  1. 1. State Key Laboratory of Magnetic Resonance and Atomic and Molecular Physics, National Center for Magnetic Resonance in Wuhan(Wuhan Institute of Physics and Mathematics, Chinese Academy of Sciences), Wuhan 430071, China;
    2. University of Chinese Academy of Sciences, Beijing 100049, China
  • Received:2016-04-19 Revised:2017-07-14 Online:2017-09-05 Published:2017-09-05

Abstract: A multi-functional spectrometer, capable of dynamic nuclear polarization (DNP) and electron paramagnetic resonance (EPR) experiments, is put forward on the basis of a home-built DNP-magnetic resonance imaging (MRI) spectrometer. A key component of the multi-functional spectrometer, microwave bridge, was designed and implemented. The microwave bridge was used to integrate the microwave transmitter of the DNP spectrometer and to enable the EPR capability. A transmitter system with high spectrum purity and dynamic range as well as a detector with low noise figure were also implemented by structure designing, circuit simulation and system evaluation. DNP and continuous wave EPR experiments were conducted to verify the reliability of the microwave bridge.

Key words: dynamic nuclear polarization (DNP), microwave bridge, low noise amplifier (LNA), electron paramagnetic resonance (EPR)

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