| [1] Lindon J C, Nicholson J K, Holmes E. The Handbook of Metabomics and Metabolomics (1st Ed)[M]. Amsterdam: Elsevier, 2007.[2] Bollard M E, Stanley E G, Lindon J C, et al. NMR-based metabonomic approaches for evaluating physiological influences on biofluid composition[J]. NMR Biomed, 2005, 18(3): 143-162.[3] Lindon J C, Nicholson J K, Holmes E, et al. Metabonomics: metabolic processes studied by NMR spectroscopy of biofluids[J]. Concepts Magn Reson, 2000, 12(5): 289-320.[4] Nicholson J K, Lindon J C, Holmes E. "Metabonomics": understanding the metabolic responses of living systems to pathophysiological stimuli via multivariate statistical analysis of biological NMR spectroscopic data[J]. Xenobiotica, 1999, 29(11): 1 181-1 189.[5] Reo N V. NMR-based metabolomics[J]. Drug Chem Toxicol, 2002, 25(4): 375-382.[6] Dunn W B, Ellis D I. Metabolomics: Current analytical platforms and methodologies[J]. Trac-Trends Anal Chem, 2005, 24(4): 285-294.[7] Bollard M E, Garrod S, Holmes E, et al. High-resolution 1H and 1H-13C magic angle spinning NMR spectroscopy of rat liver[J]. Magn Reson Med, 2000, 44(2): 201-207.[8] Garroway A N. Magic-angle sample spinning of liquids[J]. J Magn Reson, 1982, 49(1): 168-171.[9] Andrew E R, Bradbury A, Eades R G. Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation[J]. Nature, 1959, 183(4678): 1 802-1 803.[10] Lin C Y, Wu H F, Tjeerdema R S, et al. Evaluation of metabolite extraction strategies from tissue samples-using-NMR metabolomics[J]. Metabolomics, 2007, 3(1): 55-67.[11] Griffin J L, Shockcor J P. Metabolic profiles of cancer cells[J]. Nature Reviews Cancer, 2004, 4(7): 551-561.[12] Lyng H, Sitter B, Bathen T F, et al. Metabolic mapping by use of high-resolution magic angle spinning 1H MR spectroscopy for assessment of apoptosis in cervical carcinomas[J]. BMC Cancer, 2007, 7: 7-11.[13] Sitter B, Lundgren S, Bathen T F, et al. Comparison of HR MAS MR spectroscopic profiles of breast cancer tissue with clinical parameters[J]. NMR Biomed, 2006, 19(1): 30-40.[14] Zektzer A S, Swanson M G, Jarso S, et al. Improved signal to noise in high-resolution magic angle spinning total correlation spectroscopy studies of prostate tissues using rotorsynchronized adiabatic pulses[J]. Magn Reson Med, 2005, 53(1): 41-48.[15] Valonen P K, Griffin J L, Lehtimaki K K, et al. High-resolution magic-angle-spinning 1H NMR spectroscopy reveals different responses in choline-containing metabolites upon gene therapy-induced programmed cell death in rat brain glioma[J]. NMR Biomed, 2005, 18(4): 252-259.[16] Barton S J, Howe F A, Tomlins A M, et al. Comparison of in vivo 1H MRS of human brain tumours with 1H HR-MAS spectroscopy of intact biopsy samples in vitro[J]. Magn Reson Mater Phys, Biol Med, 1999, 8(2): 121-128.[17] Wang Y L, Bollard M E, Keun H, et al. Spectral editing and pattern recognition methods applied to high-resolution magic-angle spinning 1H nuclear magnetic resonance spectroscopy of liver tissues[J]. Anal Biochem, 2003, 323(1): 26-32.[18] Wang Y, Holmes E, Comelli E M, et al. Topographical variation in metabolic signatures of human gastrointestinal biopsies revealed by high-resolution magic-angle spinning 1H NMR spectroscopy[J]. J Proteome Res, 2007, 6(10): 3 944-3 951.[19] Griffin J L, Troke J, Walker L A, et al. The biochemical profile of rat testicular tissue as measured by magic angle spinning 1H NMR spectroscopy[J]. Febs Lett, 2000, 486(3): 225-229.[20] Garrod S, Humpher E, Connor S C, et al. High-resolution 1H NMR and magic angle spinning NMR spectroscopic investigation of the biochemical effects of 2-bromoethanamine in intact renal and hepatic tissue[J]. Magn Reson Med, 2001, 45(5): 781-790.[21] Cheng L L, Wu C L, Smith M R, et al. Non-destructive quantitation of spermine in human prostate tissue samples using HRMAS 1H NMR spectroscopy at 9.4 T[J]. Febs Lett, 2001, 494(1/2): 112-116.[22] Lehtimaki K K, Valonen P K, Griffin J L, et al. Metabolite changes in BT4C rat gliomas undergoing ganciclovir-thymidine kinase gene therapy-induced programmed cell death as studied by 1H NMR spectroscopy in vivo, ex vivo, and in vitro[J]. J Biol Chem, 2003, 278(46): 45 915-45 923.[23] Janssen H, Brinkmann A, van Eck E R H, et al. Microcoil high-resolution magic angle spinning NMR spectroscopy[J]. J Am Chem Soc, 2006, 128(27): 8 722-8 723.[24] Sakellariou D, Le Goff G, Jacquinot J F. High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning[J]. Nature, 2007, 447(7 145): 694-698.[25] Wong A, Aguiar P M, Sakellariou D. Slow magic-angle coil spinning: a high-sensitivity and high-resolution NMR strategy for microscopic biological specimens[J]. Magn Reson Med, 2010, 63(2): 269-274.[26] Aguiar P M, Jacquinot J F, Sakellariou D. Experimental and numerical examination of eddy (Foucault) currents in rotating micro-coils: generation of heat and its impact on sample temperature[J]. J Magn Reson, 2009, 200(1): 6-14.[27] Hoult D I, Richards R E. The signal-to-noise ratio of nuclear magnetic-resonance experiment[J]. J Magn Reson, 1976, 24(1): 71-85.[28] Terman F E. Radio Engineer's Handbook (1st Ed)[M]. New York: McGraw-Hill, 1943. 77-85.[2] Bollard M E, Stanley E G, Lindon J C, et al. NMR-based metabonomic approaches for evaluating physiological influences on biofluid composition[J]. NMR Biomed, 2005, 18(3): 143-162.[3] Lindon J C, Nicholson J K, Holmes E, et al. Metabonomics: metabolic processes studied by NMR spectroscopy of biofluids[J]. Concepts Magn Reson, 2000, 12(5): 289-320.[4] Nicholson J K, Lindon J C, Holmes E. "Metabonomics": understanding the metabolic responses of living systems to pathophysiological stimuli via multivariate statistical analysis of biological NMR spectroscopic data[J]. Xenobiotica, 1999, 29(11): 1 181-1 189.[5] Reo N V. NMR-based metabolomics[J]. Drug Chem Toxicol, 2002, 25(4): 375-382.[6] Dunn W B, Ellis D I. Metabolomics: Current analytical platforms and methodologies[J]. TracTrends Anal Chem, 2005, 24(4): 285-294.[7] Bollard M E, Garrod S, Holmes E, et al. High-resolution 1H and 1H-13 C magic angle spinning NMR spectroscopy of rat liver[J]. Magn Reson Med, 2000, 44(2): 201-207.[8] Garroway A N. Magic-angle sample spinning of liquids[J]. J Magn Reson, 1982, 49(1): 168-171.[9] Andrew E R, Bradbury A, Eades R G. Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation[J]. Nature, 1959, 183(4678): 1 802-1 803.[10] Lin C Y, Wu H F, Tjeerdema R S, et al. Evaluation of metabolite extraction strategies from tissue samples -using- NMR metabolomics[J]. Metabolomics, 2007, 3(1): 5567.[11] Griffin J L, Shockcor J P. Metabolic profiles of cancer cells[J]. Nature Reviews Cancer, 2004, 4(7): 551-561.[12] Lyng H, Sitter B, Bathen T F, et al. Metabolic mapping by use of high-resolution magic angle spinning 1H MR spectroscopy for assessment of apoptosis in cervical carcinomas[J]. BMC Cancer, 2007, 7: 7-11.[13] Sitter B, Lundgren S, Bathen T F, et al. Comparison of HR MAS MR spectroscopic profiles of breast cancer tissue with clinical parameters[J]. NMR Biomed, 2006, 19(1): 30-40.[14] Zektzer A S, Swanson M G, Jarso S, et al. Improved signal to noise in high-resolution magic angle spinning total correlation spectroscopy studies of prostate tissues using rotorsynchronized adiabatic pulses[J]. Magn Reson Med, 2005, 53(1): 41-48.[15] Valonen P K, Griffin J L, Lehtimaki K K, et al. High-resolution magic-angle-spinning 1H NMR spectroscopy reveals different responses in choline-containing metabolites upon gene therapy-induced programmed cell death in rat brain glioma[J]. NMR Biomed, 2005, 18(4): 252-259.[16] Barton S J, Howe F A, Tomlins A M, et al. Comparison of in vivo 1H MRS of human brain tumours with 1H HR-MAS spectroscopy of intact biopsy samples in vitro[J]. Magn Reson Mater Phys, Biol Med, 1999, 8(2): 121-128.[17] Wang Y L, Bollard M E, Keun H, et al. Spectral editing and pattern recognition methods applied to high-resolution magic-angle spinning 1H nuclear magnetic resonance spectroscopy of liver tissues[J]. Anal Biochem, 2003, 323(1): 26-32.[18] Wang Y, Holmes E, Comelli E M, et al. Topographical variation in metabolic signatures of human gastrointestinal biopsies revealed by high-resolution magic-angle spinning 1H NMR spectroscopy[J]. J Proteome Res, 2007, 6(10): 3 944-3 951.[19] Griffin J L, Troke J, Walker L A, et al. The biochemical profile of rat testicular tissue as measured by magic angle spinning 1H NMR spectroscopy[J]. Febs Lett, 2000, 486(3): 225-229.[20] Garrod S, Humpher E, Connor S C, et al. High-resolution 1H NMR and magic angle spinning NMR spectroscopic investigation of the biochemical effects of 2-bromoethanamine in intact renal and hepatic tissue[J]. Magn Reson Med, 2001, 45(5): 781-790.[21] Cheng L L, Wu C L, Smith M R, et al. Non-destructive quantitation of spermine in human prostate tissue samples using HRMAS 1H NMR spectroscopy at 9.4 T[J]. Febs Lett, 2001, 494(1/2): 112-116.[22] Lehtimaki K K, Valonen P K, Griffin J L, et al. Metabolite changes in BT4C rat gliomas undergoing ganciclovir-thymidine kinase gene therapy-induced programmed cell death as studied by 1H NMR spectroscopy in vivo, ex vivo, and in vitro[J]. J Biol Chem, 2003, 278(46): 45 915-45 923.[23] Janssen H, Brinkmann A, van Eck E R H, et al. Microcoil high-resolution magic angle spinning NMR spectroscopy[J]. J Am Chem Soc, 2006, 128(27): 8 722-8 723.[24] Sakellariou D, Le Goff G, Jacquinot J F. High-resolution, high-sensitivity NMR of nanolitre anisotropic samples by coil spinning[J]. Nature, 2007, 447(7 145): 694-698.[25] Wong A, Aguiar P M, Sakellariou D. Slow magic-angle coil spinning: a high-sensitivity and high-resolution NMR strategy for microscopic biological specimens[J]. Magn Reson Med, 2010, 63(2): 269-274.[26] Aguiar P M, Jacquinot J F, Sakellariou D. Experimental and numerical examination of eddy (Foucault) currents in rotating micro-coils: generation of heat and its impact on sample temperature[J]. J Magn Reson, 2009, 200(1): 6-14.[27] Hoult D I, Richards R E. The signal-to-noise ratio of nuclear magnetic-resonance experiment[J]. J Magn Reson, 1976, 24(1): 71-85.[28] Terman F E. Radio Engineer's Handbook (1st Ed)[M]. New York: McGraw-Hill, 1943. 77-85. |
