An ARM-Based Variable-Temperature and Sample Handling Pneumatics System for NMR Spectrometers

Abstract

Abstract:

A variable-temperature and sample handling pneumatics system was designed for NMR spectrometer. An ARM with CAN controller is used as the center processor of the system, which controls the airflow and temperature through PID control algorithm. The controller of the design can carry out changing or spinning sample and variable-temperature. This design has many other benefits, including easy control, high precision and low cost.

Key words: NMR, sample handling pneumatics, variable-temperature, PID

CLC Number:

O482.53

ZHANG Zhi, LIU Hai-Dan, LI You, MAO Wen-Ping, LIU Chao-Yang, QIU Jian-Qing . An ARM-Based Variable-Temperature and Sample Handling Pneumatics System for NMR Spectrometers[J]. Chinese Journal of Magnetic Resonance, 2011, 28(1): 50-58.

References

[1] Wang Jin-shan（王金山）．NMR Spectrometer and Experiment Technology(核磁共振波谱仪与实验技术)[M]．Beijing(北京)： Machinery Industry Press（机械工业出版社），1982.

[2] Li Ning（李宁）．Development and Application of the MDK-Based STM32 Processor（基于MDK的STM32处理器开发应用）[M]．Beijing(北京)：Beijing University of Aeronautics and Astronautics Press（北京航空航天大学出版社)，2008.

[3] Wang Yong-hong（王永虹），Xu Wei（徐炜），Hao Li-ping（郝立平）．Theory and Practice of the ARM Cortex——M3 Microprocessors of STM32 Series（STM32系列ARM Cortex——M3微控制器原理与实践）[M]．Beijing(北京)： Beijing University of Aeronautics and Astronautics Press (北京航空航天大学出版社)，2008.

[4] Sun De-bao（孙德宝），Wang Yong-ji（王永骥），Wang Jin-cheng（王金城）．Automatic Control Theory（自动控制原理）[M]．Beijing(北京)：Chemistry Industry Press（化学工业出版社），2002.

[5] Wang Wen-juan(王文娟)，Hu Peng(胡鹏)，Mao Wen-ping(毛文平)，et al. An ARM and CPLD-based preamplifier control system for NMR spectrometer (基于ARM和CPLD的NMR谱仪前放控制器) [J]. Chinese J Magn Reson(波谱学杂志)，2009，26(3): 351-358. 

[6] Kang Hua-guang（康华光）．Basic of Electronic Technology·Digital Section（电子技术基础·数字部分）[M]．Beijing(北京)：Higher Education Press (高等教育出版社)，2000.

[7] Linear Technology Corporation．LTC2600_Datasheet[EB/OL]．2003.

[8] Kang Hua-guang（康华光）．Basic of Electronic Technology·Analog Section（电子技术基础·模拟部分）[M]．Beijing(北京)：Higher Education Press（高等教育出版社），2000.

[9] Jia Bo-nian（贾伯年），Yu Pu（俞朴），Song Ai-guo（宋爱国）. Sensor Technology（传感器技术）[M]．Nanjing(南京)：Southeast University Press(东南大学出版社)，2007.

[10] Ren Zhi(任智）, Zhang Zhi(张志). Test and calibration of temperature control system in NMR spectrometer (NMR仪器温控系统测试与校正)[J]. Analysis and Testing Technology and Instruments(分析测试技术与仪器), 2010, 16(3): 146-151.

[11] Texas Instruments Incorporated．ADS1258_Datasheet[EB/OL]．2003.

[12] Jiang Ting-ting(姜婷婷)，Chen Yi-qun(陈义群)，Fang Hui-ru(方惠如)，et al. Multi-layer architecture design of software used on NMR spectrometer console(一种NMR谱仪控制台软件系统的多层架构设计)[J]. Chinese J Magn Reson(波谱学杂志)，2009，26(4): 497-503.

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