Chinese Journal of Magnetic Resonance ›› 2017, Vol. 34 ›› Issue (2): 231-244.doi: 10.11938/cjmr20170213
Previous Articles Next Articles
ZHANG Zhen1,2, HE Yu-gui1, HUANG Chong-yang1, LIU Chao-yang1, FENG Ji-wen1
Received:
2016-04-13
Revised:
2017-04-15
Online:
2017-06-05
Published:
2017-06-05
CLC Number:
ZHANG Zhen, HE Yu-gui, HUANG Chong-yang, LIU Chao-yang, FENG Ji-wen. A Review on Microwave-Induced Optical Nuclear Polarization[J]. Chinese Journal of Magnetic Resonance, 2017, 34(2): 231-244.
[1] GERSHENFELD N A, CHUANG I L. Bulk spin-resonance quantum computation[J]. Science, 1997, 275(5298):350-356. [2] PENG X H, SUTER D. Spin qubits for quantum simulations[J]. Front Phys China, 2010, 5(1):1-25. [3] LI Z K, ZHOU H, JU C Y, et al. Experimental realization of a compressed quantum simulation of a 32-spin Ising chain[J]. Phys Rev Lett, 2014, 112(22):220501. [4] VLAARDINGERBROEK M T, BOER J A. Magnetic resonance imaging[M]. 2nd ed. Berlin:Springer-Verlag, 1999. [5] TAKEDA K. Studies on dynamic nuclear polarization using photo-excited triplet electron spins[D]. Kyoto:Kyoto University, 2003. [6] CHERUBINI A, PAYNE G, LEACH M, et al. Hyperpolarising 13C for NMR studies using laser-polarised 129Xe:SPINOE vs thermal mixing[J]. Chem Phys Lett, 2003, 371(5):640-644. [7] LI H D, ZHAN Z Y, HAN Y Q, et al. Lung MRI use Hyperpolarized gase[J]. Chinese J Magn Reson, 2014, 31(3):307-320. 李海东, 张智颖, 韩叶清, 等. 超级化气体肺部磁共振成像[J]. 波谱学杂志, 2014, 31(3):307-320. [8] GOLMAN K, AXELSSON O, JÓHANNESSON H, et al. Parahydrogen-induced polarization in imaging:Subsecond 13C angiography[J]. Magn Reson Med, 2001, 46(1):1-5. [9] BLÄTTLER C, JENT F, PAUL H. A novel radical-triplet pair mechanism for chemically induced electron polarization (CIDEP) of free radicals in solution[J]. Chem Phys Lett, 1990, 166(4):375-380. [10] OVERHAUSER A W. Paramagnetic relaxation in metals[J]. Physical Review, 1953, 89(4):689-790. [11] LUMATA L L, MARTIN R, JINDAL A K, et al. Development and performance of a 129-GHz dynamic nuclear polarizer in an ultra-wide bore superconducting magnet[J]. MAGMA, 2015, 28(2):195-205. [12] POLYON C, LURIE D, YOUNGDEE W, et al. Field-cycled dynamic nuclear polarization (FC-DNP) of 14N and 15N nitroxide radicals at low magnetic field[J]. J Phys D Appl Phys, 2007, 40(18):5527-5532. [13] NEUDERT O, MATTEA C, STAPF S, et al. Fast-field-cycling relaxometry enhanced by dynamic nuclear polarization[J]. Micropor Mesopor Mat, 2015, 205:70-74. [14] JANNIN S, COMMENT A, KURDZESAU F, et al. A 140 GHz prepolarizer for dissolution dynamic nuclear polarization[J]. J Chem Phys, 2008, 128(24):241102. [15] JANNIN S, BORNET A, COLOMBO S, et al. Low-temperature cross polarization in view of enhancing dissolution dynamic nuclear polarization in NMR[J]. Chem Phys Lett, 2011, 517(4):234-236. [16] HAZE O, CORZILIUS B R, SMITH A A, et al. Water-soluble narrow-line radicals for dynamic nuclear polarization[J]. J Am Chem Soc, 2012, 134(35):14287-14290. [17] ZHOU J W, LI L Y, HU H B, et al. Study of natural diamonds by dynamic nuclear polarization-enhanced 13C nuclear magnetic resonance spectroscopy[J]. Solid State Nucl Magn Reson, 1994, 3(6):339-351. [18] HE Y G, FENG J W, ZHANG Z, et al. Development of pulsed dynamic nuclear polarization for enhancing NMR and MRI[J]. Chinese J Magn Reson, 2015, 32(2):393-398. 贺玉贵, 冯继文, 张志, 等. 脉冲动态核极化增强的NMR和MRI系统研究[J]. 波谱学杂志, 2015, 32(2):393-398. [19] HE Y G, FENG J W, ZHANG Z, et al. A peripheral component interconnect express-based scalable and highly integrated pulsed spectrometer for solution state dynamic nuclear polarization[J]. Rev Sci Instrum, 2015, 86(8):083101. [20] HE Y G, ZHANG Z, FENG J W, et al. Simultaneous acquisition of multi-nuclei enhanced NMR/MRI by solution state dynamic nuclear polarization[J]. Sci China Chem, 2016, 59(7):830-835. [21] MAIER G, HAEBERLEN U, WOLF H, et al. Optische kernspin-polarisation in anthracen-kristallen[J]. Phys Lett A, 1967, 25(5):384-385. [22] GROVER B. Noble-gas NMR detection through noble-gas-rubidium hyperfine contact interaction[J]. Phys Rev Lett, 1978, 40(6):391-392. [23] JEFFRIES C. Some new schemes for polarizing nuclei[J]. Phys Rev Lett, 1967, 19(21):1221-1224. [24] LAMPEL G. Nuclear dynamic polarization by optical electronic saturation and optical pumping in semiconductors[J]. Phys Rev Lett, 1968, 20(10):491-493. [25] DEIMLING M, BRUNNER H, DINSE K, et al. Microwave-induced optical nuclear polarization (MI-ONP)[J]. J Magn Reson, 1980, 39(2):185-202. [26] HENSTRA A, LIN T S, SCHMIDT J, et al. High dynamic nuclear polarization at room temperature[J]. Chem Phys Lett, 1990, 165(1):6-10. [27] KAGAWA A, NEGORO M, TAKEDA K, et al. Magnetic-field cycling instrumentation for dynamic nuclear polarization-nuclear magnetic resonance using photoexcited triplets[J]. Rev Sci Instrum, 2009, 80(4):044705. [28] ⅡNUMA M. Dynamic nuclear polarization at high temperature for polarized proton target[D]. Kyoto:Kyoto University, 1997. [29] ⅡNUMA M, TAKAHASHI Y, SHAKÉ I, et al. High proton polarization by microwave-induced optical nuclear polarization at 77 K[J]. Phys Rev Lett, 2000, 84(1):171. [30] BLOEMBERGEN N. On the interaction of nuclear spins in a crystalline lattice[J]. Physica, 1949, 15(3):386-426. [31] KAGAWA A, MUROKAWA Y, TAKEDA K, et al. Optimization of 1H spin density for dynamic nuclear polarization using photo-excited triplet electron spins[J]. J Magn Reson, 2009, 197(1):9-13. [32] HENSTRA A, DIRKSEN P, SCHMIDT J, et al. Nuclear spin orientation via electron spin locking (NOVEL)[J]. J Magn Reson, 1988, 77(2):389-393. [33] HAUSSER K. Optical spin polarization in molecular crystals[J]. Pure Appl Chem, 1972, 32(1-4):183-196. [34] YANG T C, SLOOP D J, WEISSMAN S, et al. Zero-field magnetic resonance of the photo-excited triplet state of pentacene at room temperature[J]. J Chem Phys, 2000, 113(24):11194-11201. [35] SLOOP D J, YU H L, LIN T S, et al. Electron spin echoes of a photoexcited triplet:Pentacene in p-terphenyl crystals[J]. J Chem Phys, 1981, 75(8):3746-3757. [36] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by electron spins in the photoexcited triplet state:Ⅱ. High polarization of the residual protons in deuterated naphthalene[J]. J Phys Soc Jpn, 2004, 73(8):2319-2322. [37] MCCONNELL H M, CHESNUT D B. Theory of isotropic hyperfine interactions in π-electron radicals[J]. J Chem Phys, 1958, 28(1):107-117. [38] WENCKEBACH W T. The solid effect[J]. Appl Magn Reson, 2008, 34(3, 4):227-235. [39] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by electron spins in the photoexcited triplet state:I. Attainment of proton polarization of 0.7 at 105 K in naphthalene[J]. J Phys Soc Jpn, 2004, 73(8):2313-2318. [40] VAN KESTEREN H, WENCKEBACH W T, SCHMIDT J. The mechanism of microwave-induced optical nuclear polarization in fluorene doped with phenanthrene:A qualitative analysis[J]. Chem Phys Lett, 1985, 121(4):440-445. [41] VAN KESTEREN H, WENCKEBACH W T, SCHMIDT J. The mechanism of microwave induced optical nuclear polarization in the system fluorene doped with phenanthrene:A quantitative analysis[J]. Mol Phys, 1986, 58(2):263-271. [42] PENFOLD J, WARD R, WILLIAMS W. A time-of-flight neutron reflectometer for surface and interfacial studies[J]. J Phys E Sci Instrum, 1987, 20(11):1411-1417. [43] VERHEIJ P F, WENCKEBACH W T, SCHMIDT J. Microwave induced optical nuclear polarization at 75 GHz:A quantitative analysis[J]. Appl Magn Reson, 1993, 5(2):187-205. [44] EICHHORN T R, HAAG M, VAN DEN BRANDT B, et al. An apparatus for pulsed ESR and DNP experiments using optically excited triplet states down to liquid helium temperatures[J]. J Magn Reson, 2013, 234:58-66. [45] EICHHORN T, BRANDT BVD, HAUTLE P, et al. Dynamic nuclear polarisation via the integrated solid effect Ⅱ:experiments on naphthalene-h 8 doped with pentacene-d14[J]. Mol Phys, 2014, 112(13):1773-1782. [46] ⅡNUMA M, SHAKÉ I, TAKIZAWA R, et al. High proton polarization in crystalline naphthalene by dynamic nuclear polarization with laser excitation at room temperature and liquid nitrogen temperature[J]. Phys Lett A, 1995, 208(3):251-256. [47] TAKEDA K, YAMAMURA T, KAGAWA A, et al. Enhancement of efficiency in photo-excitation to the triplet state by laser-pulse reshaping[J]. J Magn Reson, 2005, 174(2):310-313. [48] TAKEDA K, TAKEGOSHI K, TERAO T. Zero-field electron spin resonance and theoretical studies of light penetration into single crystal and polycrystalline material doped with molecules photoexcitable to the triplet state via intersystem crossing[J]. J Chem Phys, 2002, 117(10):4940-4946. [49] ALLGEIER J, BUNTKOWSKY G, HENTRICH S, et al. Optical nuclear polarization of deuterium spins:mechanisms and applications in solid state NMR[J]. Isr J Chem, 1992, 32(2, 3):205-213. [50] TAKEDA K, TAKEGOSHI K, TERAO T. Dynamic nuclear polarization by photoexcited-triplet electron spins in polycrystalline samples[J]. Chem Phys Lett, 2001, 345(1):166-170. [51] TATEISHI K, NEGORO M, KAGAWA A, et al. Hyperpolarization of thin films with dynamic nuclear polarization using photoexcited triplet electrons[J]. J Phys Soc Jpn, 2013, 82(8):084005. [52] TATEISHI K, NEGORO M, KAGAWA A, et al. Dynamic nuclear polarization with photoexcited triplet electrons in a glassy matrix[J]. Angew Chem, 2013, 125(50):13549-13552. [53] SAKAGUCHI S, UESAKA T, KAWAHARA T, et al. Proton polarization in photo-excited aromatic molecule at room temperature enhanced by intense optical source and temperature control[J]. Nuclear Instru and Meth Phys Res B:Beam Interactions with Materials and Atoms, 2013, 317:679-684. [54] KAWAHARA T, SAKAGUCHI S, TATEISHI K, et al. Kinetic parameters of photo-excited triplet state of pentacene determined by dynamic nuclear polarization[J]. J Phys Soc Jpn, 2015, 84(4):044005. [55] TATEISHI K, NEGORO M, NISHIDA S, et al. Room temperature hyperpolarization of nuclear spins in bulk[J]. P Natl Acad Sci USA, 2014, 111(21):7527-7530. [56] NEGORO M, NAKAYAMA K, TATEISHI K, et al. 2H-decoupling-accelerated 1H spin diffusion in dynamic nuclear polarization with photoexcited triplet electrons[J]. J Chem Phys, 2010, 133(15):154504. [57] EICHHORN T, HAAG M, VAN DEN BRANDT B, et al. High proton spin polarization with DNP using the triplet state of pentacene-d14[J]. Chem Phys Lett, 2013, 555:296-299. [58] ⅡNUMA M, TAKAHASHI Y, SHAKÉ I, et al. Proton polarization with p-terphenyl crystal by integrated solid effect on photoexcited triplet state[J]. J Magn Reson, 2005, 175(2):235-241. [59] PINES A, GIBBY M, WAUGH J. Proton-enhanced NMR of dilute spins in solids[J]. J Chem Phys, 1973, 59(2):569-590. |
[1] | ZHAO Shang-yi WANG Yuan-jun. Classification of Alzheimer's Disease Patient and Healthy Group Based on Magnetic Resonance Images and Improved UNet++ Model [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[2] | LU Chen DONG Jian-jian ZHONG Kai. TX Mice Brain Study with Diffusion Tensor Imaging at 9.4 T [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[3] | WANG Ke ZHANG Ying-hua LI Yu-qing ZOU Ding-hua. Application of Solid State Nuclear Magnetic Resonance Spectroscopy in Cementitious Materials Research [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[4] |
LIU Ke-wen LIU Zi-long WANG Xiang-yu CHEN Li LI Zhao WU Guang-yao LIU Chao-yang.
Prostate Cancer Diagnosis based on Cascaded Convolutional Neural Networks [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[5] | YAN Song TU Xiao-qing PENG Mei. Design and Implementation of Monitoring System for Polarization Degree of Optical Pumping 3He [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[6] | ZHANG Yi-ming CHEN Zhi-xue YANG Xiao-yun. Spectral Analysis and Structural Elucidation of Cyflumetofen [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[7] | WANG Qiang WEI Shu-feng WANG Zheng YANG Wen-hui. The Optimal Design of Matrix Gradient Coils Based on Particle Swarm Optimization and Genetic Algorithm [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[8] | WANG Jia-xin FENG Ji-wen CHEN Jun-fei WANG Li-ying LIU Chao-yang. Research and Implementation on Magic Angle Spinning Rotor for Solid State Nuclear Magnetic Resonance Probe [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[9] | ZHAO Zhi-hui LIU Biao-lan YAN Xiao-shuang WU Shuai-shuai RU Ge-ying MAO Shi-zhen Feng Ji-wen. NMR Studies on Thermally Triggered Self-Assembly of PSSS50-b-PNIPAM300 in Binary Solvent [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[10] | . Preparation of Singlet States and Analysis of Influencing Factors on Their Transfer Efficiency and Lifetime [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[11] | . Process in Solid-State NMR Studies of Carbon Anode Materials for Lithium/Sodium-ion Batteries [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[12] | . 13C Chemical Shift Assignment of Solid 2-Picolinic Acid by DFT/Crystallography Integrated Approach [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[13] | . A Design for Discontinuous Microwave Inquiry Signal Generation [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[14] | ZHANG Fen-fen SHEN Wen-bin XU Kai-bing YANG Ming. Quantitative Analysis for Ticagrelor Based on Proton Nuclear Magnetic Resonance [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[15] | XU Guang-yong DONG Man-yuan MA Jian-feng ZHANG Li-min. A Solid State NMR study of Molecular Dynamics of Semi-Crystalline Poly(3-Hydroxybutyrate) And Poly(3-Hydroxybutyrate-Co-3-Hydroxyvalerate) [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||