Chinese Journal of Magnetic Resonance ›› 2016, Vol. 33 ›› Issue (3): 361-367.doi: 10.11938/cjmr20160301
Previous Articles Next Articles
YAN Xiao-jing, HU Bing-wen
Received:
2015-03-11
Revised:
2016-07-15
Online:
2016-09-05
Published:
2016-09-05
Supported by:
Large Instruments Open Foundation of East China Normal University, National Natural Science Foundation of China (21373086), National Science Fund of China for Excellent Young Scholars (21522303), Basic Research Project of Shanghai Science and Technology Committee (14JC1491000).
CLC Number:
YAN Xiao-jing, HU Bing-wen. Probing 15N-15N Correlations in g-C3N4 Samples with Solid-State NMR SHA+ Pulse Sequence[J]. Chinese Journal of Magnetic Resonance, 2016, 33(3): 361-367.
[1] Castellani F, van Rossum B, Diehl A, et al. Structure of a protein determined by solid-state magic-angle-spinning NMR spectroscopy[J]. Nature, 2002, 420(6 911): 98-102.[2] Lange A, Becker S, Seidel K, et al. A concept for rapid protein-structure determination by solid-state NMR spectroscopy[J]. Angew Chem Int Ed Engl, 2005, 44(14): 2 089-2 092.[3] Wasmer C, Lange A, van Melckebeke H, et al. Amyloid fibrils of the HET-s (218-289) Prion form a b solenoid with a triangular hydrophobic core[J]. Science, 2008, 319(5 869): 1 523-1 526.[4] Lange A, Giller K, Hornig S, et al. Toxin-induced conformational changes in a potassium channel revealed by solid-state NMR[J]. Nature, 2006, 440(7 086): 959-962.[5] Renault M, Cukkemane A, Baldus M. Solid-state NMR spectroscopy on complex biomolecules[J]. Angew Chem Int Ed Engl, 2010, 49(45): 8 346-8 357.[6] Hong M, Zhang Y, Hu F H. Membrane protein structure and dynamics from NMR spectroscopy[J]. Annu Rev Phys Chem, 2012, 63: 1-24.[7] Tycko R. Solid-state NMR studies of amyloid fibril structure[J]. Annu Rep Phys Chem, 2011, 62: 279-299.[8] Takegoshi K, Nakamura S, Terao T. 13C-1H dipolar-assisted rotational resonance in magic-angle spinning NMR[J]. Chem Phys Lett, 2001, 344(5): 631-637.[9] Takegoshi K, Nakamura S, Terao T. 13C-1H dipolar-driven 13C-13C recoupling without 13C rf irradiation in nuclear magnetic resonance of rotating solids[J]. J Chem Phys, 2003, 118(5): 2 325-2 341.[10] Weingarth M, Masuda Y, Takegoshi K, et al. Sensitive 13C-13C correlation spectra of amyloid fibrils at very high spinning frequencies and magnetic fields[J]. J Biomol NMR, 2011, 50(2): 129-136.[11] Weingarth M, Bodenhausen G, Tekely P. Broadband carbon-13 correlation spectra of micro crystalline proteins in very high-magnetic fields[J]. J Am Chem Soc, 2009, 131(39): 13 937-13 939.[12] Weingarth M, Demco D E, Bodenhausen G, et al. Improved magnetization transfer in solid-state NMR with fast magic angle spinning[J]. Chem Phys Lett, 2009, 469(4, 5, 6): 342-348.[13] Hu B W, Lafon O, Trébosc J, et al. Broad-band homo-nuclear correlations assisted by 1H irradiation for bio-molecules in very high magnetic field at fast and ultra-fast MAS frequencies[J]. J Magn Reson, 2011, 212(2): 320-329.[14] Hu B W, Trébosc J, Lafon O, et al. Very-long-distance correlations in proteins revealed by solid-state NMR spectroscopy[J]. Chem Phys Chem, 2012, 13(16): 3 585-3 588.[15] Scholz I, van Beek J D, Ernst M. Operator-based Floquet theory in solid-state NMR[J]. Solid State Nucl Magn Reson, 2010, 37(3, 4): 39-59.[16] Leskes M, Akbey Ü, Oschkinat H, et al. Radio frequency assisted homo-nuclear recoupling, a Floquet description of homo-nuclear recoupling via surrounding hetero-nuclei in fully protonated to fully deuterated systems[J]. J Magn Reson, 2011, 209(2): 207-219.[17] Jurgens B, Irran E, Senker J, et al. Melem (2,5,8-Triamino-tri-s-triazine), an important intermediate during condensation of melamine rings to Graphitic Carbon Nitride: synthesis, structure determination by X-ray powder diffractometry, solid-state NMR, and theoretical studies[J]. J Am Chem Soc, 2003, 125(34): 10 288-10 300.[18] Bak M, Rasmussen J T, Nielsen N C. SIMPSON: A general simulation program for solid-state NMR spectroscopy[J]. J Magn Reson, 2000, 147(2): 296-330.[19] Bak M, Nielsen N C. REPULSION: A novel approach to efficient powder averaging in solid-state NMR[J]. J Magn Reson, 1997, 125(1): 132-139.[20] Fung B M, Khitrin A K, Ermolaev K. An improved broadband decoupling sequence for liquid crystals and solids[J]. J Magn Reson, 2000, 142(1): 97-101.[21] Lotsch B V, Dçblinger M, Sehnert J, et al. Unmasking melon by a complementary approach employing electron diffraction, solid-state NMR spectroscopy, and theoretical calculations; structural characterization of a carbon nitride polymer[J]. Chem Eur J, 2007, 13(17): 4 969-4 980.[22] Vosegaard T. Challenges in numerical simulations of solid-state NMR experiments: Spin exchange pulse sequences[J]. Solid State Nucl Magn Reson, 2010, 38(4): 77-83. |
[1] | ZHAO Shang-yi WANG Yuan-jun. Classification of Alzheimer's Disease Patient and Healthy Group Based on Magnetic Resonance Images and Improved UNet++ Model [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[2] | LU Chen DONG Jian-jian ZHONG Kai. TX Mice Brain Study with Diffusion Tensor Imaging at 9.4 T [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[3] | WANG Ke ZHANG Ying-hua LI Yu-qing ZOU Ding-hua. Application of Solid State Nuclear Magnetic Resonance Spectroscopy in Cementitious Materials Research [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[4] |
LIU Ke-wen LIU Zi-long WANG Xiang-yu CHEN Li LI Zhao WU Guang-yao LIU Chao-yang.
Prostate Cancer Diagnosis based on Cascaded Convolutional Neural Networks [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[5] | YAN Song TU Xiao-qing PENG Mei. Design and Implementation of Monitoring System for Polarization Degree of Optical Pumping 3He [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[6] | ZHANG Yi-ming CHEN Zhi-xue YANG Xiao-yun. Spectral Analysis and Structural Elucidation of Cyflumetofen [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[7] | WANG Qiang WEI Shu-feng WANG Zheng YANG Wen-hui. The Optimal Design of Matrix Gradient Coils Based on Particle Swarm Optimization and Genetic Algorithm [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[8] | WANG Jia-xin FENG Ji-wen CHEN Jun-fei WANG Li-ying LIU Chao-yang. Research and Implementation on Magic Angle Spinning Rotor for Solid State Nuclear Magnetic Resonance Probe [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[9] | ZHAO Zhi-hui LIU Biao-lan YAN Xiao-shuang WU Shuai-shuai RU Ge-ying MAO Shi-zhen Feng Ji-wen. NMR Studies on Thermally Triggered Self-Assembly of PSSS50-b-PNIPAM300 in Binary Solvent [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[10] | . Preparation of Singlet States and Analysis of Influencing Factors on Their Transfer Efficiency and Lifetime [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[11] | . Process in Solid-State NMR Studies of Carbon Anode Materials for Lithium/Sodium-ion Batteries [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[12] | . 13C Chemical Shift Assignment of Solid 2-Picolinic Acid by DFT/Crystallography Integrated Approach [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[13] | . A Design for Discontinuous Microwave Inquiry Signal Generation [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[14] | ZHANG Fen-fen SHEN Wen-bin XU Kai-bing YANG Ming. Quantitative Analysis for Ticagrelor Based on Proton Nuclear Magnetic Resonance [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
[15] | XU Guang-yong DONG Man-yuan MA Jian-feng ZHANG Li-min. A Solid State NMR study of Molecular Dynamics of Semi-Crystalline Poly(3-Hydroxybutyrate) And Poly(3-Hydroxybutyrate-Co-3-Hydroxyvalerate) [J]. Chinese Journal of Magnetic Resonance, 0, (): 0-0. |
Viewed | ||||||
Full text |
|
|||||
Abstract |
|
|||||