绿柱虫二萜二醇A在手性位移试剂Eu(tfc)3存在下的1H-NMR研究

波谱学杂志 ›› 1991, Vol. 8 ›› Issue (4): 465-468.

绿柱虫二萜二醇A在手性位移试剂Eu(tfc)₃存在下的¹H-NMR研究

王小霞¹, 钟永利², 苏镜娱²

1. 中山大学测试中心广州 510275;
2. 中山大学化学系广州 510275

收稿日期:1991-01-16 修回日期:1991-04-01 出版日期:1991-12-05 发布日期:2018-01-20
基金资助:
国家自然科学基金资助课题

STUDY ON THE ¹H-NMR SPECTRUM OF CLAVUDIOL A IN THE EXISTENCE OF CHIRAL SHIFT REAGENT

Wang Xiaoxia¹, Zhong Yongli², Su Jingyu²

1. Instrumentation Analysis and Research Centre, Zhongshan University, Guangzhou;
2. Department of Chemistry, Zhongshan University, Guangzhou

Received:1991-01-16 Revised:1991-04-01 Online:1991-12-05 Published:2018-01-20

摘要/Abstract

摘要： 本文研究了在手性位移试剂Eu(tfc)₃存在下,绿柱虫二萜二醇A(clavudiol A)(1)中各甲基的化学位移变化,并对19-甲基和20-甲基的¹H-NMR进行了归属。

关键词: 绿柱虫二萜二醇A, 手性位移试剂Eu(tfc)₃, ¹H-NMR研究

Abstract: The ¹H-NMR spectrum of clavudiol A (1) has been studied in the existence of chiral reagent Eu (tfc)₃. In addition, the chemical shifts of 19-methyl and 20-methyl of 1 was determined by ¹H-NMR spectrum.

Key words: Clavudiol A, Chiral shift reagent Eu (tfc)₃, ¹H-NMR study

王小霞, 钟永利, 苏镜娱. 绿柱虫二萜二醇A在手性位移试剂Eu(tfc)₃存在下的¹H-NMR研究[J]. 波谱学杂志, 1991, 8(4): 465-468.

Wang Xiaoxia, Zhong Yongli, Su Jingyu. STUDY ON THE ¹H-NMR SPECTRUM OF CLAVUDIOL A IN THE EXISTENCE OF CHIRAL SHIFT REAGENT[J]. Chinese Journal of Magnetic Resonance, 1991, 8(4): 465-468.

绿柱虫二萜二醇A在手性位移试剂Eu(tfc)₃存在下的¹H-NMR研究

STUDY ON THE ¹H-NMR SPECTRUM OF CLAVUDIOL A IN THE EXISTENCE OF CHIRAL SHIFT REAGENT

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